N-Phenyl-N-(3,4,4-trichlorobut-3-en-1-yn-1-yl)aniline

Base Information

Chemical Name:N-Phenyl-N-(3,4,4-trichlorobut-3-en-1-yn-1-yl)aniline
CAS No.:82505-77-9
Molecular Formula:C₁₆H₁₀Cl₃N
Molecular Weight:322.621
Hs Code.:
DSSTox Substance ID:DTXSID30512888

Synonyms:82505-77-9;DTXSID30512888;N-Phenyl-N-(3,4,4-trichlorobut-3-en-1-yn-1-yl)aniline

Suppliers and Price of N-Phenyl-N-(3,4,4-trichlorobut-3-en-1-yn-1-yl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-Phenyl-N-(3,4,4-trichlorobut-3-en-1-yn-1-yl)aniline

Chemical Property:

XLogP3:6.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:320.987882
Heavy Atom Count:20
Complexity:384

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)N(C#CC(=C(Cl)Cl)Cl)C2=CC=CC=C2

Technology Process of N-Phenyl-N-(3,4,4-trichlorobut-3-en-1-yn-1-yl)aniline

There total 1 articles about N-Phenyl-N-(3,4,4-trichlorobut-3-en-1-yn-1-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5658-91-3
1,1,2,4-tetrachloro-1-buten-3-yne

: 122-39-4
diphenylamine

: 82505-77-9
N,N-Diphenyl-N-(3,4,4-trichlor-3-buten-1-inyl)amin

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) THF, Et₂O, hexane, 1 h, RT; 2) THF, hexane, Et₂O, 10 min, -25 deg C; 2 h, RT;
DOI:10.1002/hlca.19880710810

Reference yield:

: 82505-77-9
N,N-Diphenyl-N-(3,4,4-trichlor-3-buten-1-inyl)amin

: 86895-99-0
N,N-Diphenyl-4-(piperidino)butadiinamin

Guidance literature:: Multi-step reaction with 2 steps

1: BuLi, Bromcyan / 2 h, room temp. than 1 h, 0 deg C

2: 54 percent / diethyl ether / 15 h / Ambient temperature

With n-butyllithium; bromocyane; In diethyl ether;
DOI:10.1016/S0040-4039(00)81872-9

Reference yield:

: 82505-77-9
N,N-Diphenyl-N-(3,4,4-trichlor-3-buten-1-inyl)amin

: 86896-00-6
(4-Morpholin-4-yl-buta-1,3-diynyl)-diphenyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: BuLi, Bromcyan / 2 h, room temp. than 1 h, 0 deg C

2: 56 percent / diethyl ether / 15 h / Ambient temperature

With n-butyllithium; bromocyane; In diethyl ether;
DOI:10.1016/S0040-4039(00)81872-9