L-Phenylalaninamide, N-[(1,1-dimethylethoxy)carbonyl]-L-alanyl-L-alanyl-N-[(1S)-1-[(3R,4S)-1-[ (1S)-1-(methoxycarbonyl)-3-methylbutyl]-2-oxo-4-phenyl-3-azetidinyl]eth yl]-

Base Information

Chemical Name:L-Phenylalaninamide, N-[(1,1-dimethylethoxy)carbonyl]-L-alanyl-L-alanyl-N-[(1S)-1-[(3R,4S)-1-[ (1S)-1-(methoxycarbonyl)-3-methylbutyl]-2-oxo-4-phenyl-3-azetidinyl]eth yl]-
CAS No.:825615-51-8
Molecular Formula:C₃₈H₅₃N₅O₈
Molecular Weight:707.868
Hs Code.:

L-Phenylalaninamide,
N-[(1,1-dimethylethoxy)carbonyl]-L-alanyl-L-alanyl-N-[(1S)-1-[(3R,4S)-1-[
(1S)-1-(methoxycarbonyl)-3-methylbutyl]-2-oxo-4-phenyl-3-azetidinyl]eth
yl]-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-Phenylalaninamide, N-[(1,1-dimethylethoxy)carbonyl]-L-alanyl-L-alanyl-N-[(1S)-1-[(3R,4S)-1-[ (1S)-1-(methoxycarbonyl)-3-methylbutyl]-2-oxo-4-phenyl-3-azetidinyl]eth yl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of L-Phenylalaninamide, N-[(1,1-dimethylethoxy)carbonyl]-L-alanyl-L-alanyl-N-[(1S)-1-[(3R,4S)-1-[ (1S)-1-(methoxycarbonyl)-3-methylbutyl]-2-oxo-4-phenyl-3-azetidinyl]eth yl]-

There total 6 articles about L-Phenylalaninamide, N-[(1,1-dimethylethoxy)carbonyl]-L-alanyl-L-alanyl-N-[(1S)-1-[(3R,4S)-1-[ (1S)-1-(methoxycarbonyl)-3-methylbutyl]-2-oxo-4-phenyl-3-azetidinyl]eth yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2666-93-5
(S)-Leu-OMe

: 825615-51-8
(S)-2-[(3R,4S)-3-((S)-1-{(S)-2-[(S)-2-((S)-2-tert-Butoxycarbonylamino-propionylamino)-propionylamino]-3-phenyl-propionylamino}-ethyl)-2-oxo-4-phenyl-azetidin-1-yl]-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 3 h / 20 °C

2: 15 percent / diethyl ether / 1.5 h / -30 °C / UV-irradiation

3: Et₂NH / acetonitrile / 0.5 h / 20 °C

4: 177 mg / CH₂Cl₂ / 2.5 h / 20 °C

With diethylamine; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200400295

Reference yield:

: 75691-28-0
methyl (S)-2-(benzylideneamino)-4-methylpentanoate

: 825615-51-8
(S)-2-[(3R,4S)-3-((S)-1-{(S)-2-[(S)-2-((S)-2-tert-Butoxycarbonylamino-propionylamino)-propionylamino]-3-phenyl-propionylamino}-ethyl)-2-oxo-4-phenyl-azetidin-1-yl]-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 15 percent / diethyl ether / 1.5 h / -30 °C / UV-irradiation

2: Et₂NH / acetonitrile / 0.5 h / 20 °C

3: 177 mg / CH₂Cl₂ / 2.5 h / 20 °C

With diethylamine; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200400295

Reference yield:

: 100-52-7
benzaldehyde

: 825615-51-8
(S)-2-[(3R,4S)-3-((S)-1-{(S)-2-[(S)-2-((S)-2-tert-Butoxycarbonylamino-propionylamino)-propionylamino]-3-phenyl-propionylamino}-ethyl)-2-oxo-4-phenyl-azetidin-1-yl]-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 3 h / 20 °C

2: 15 percent / diethyl ether / 1.5 h / -30 °C / UV-irradiation

3: Et₂NH / acetonitrile / 0.5 h / 20 °C

4: 177 mg / CH₂Cl₂ / 2.5 h / 20 °C

With diethylamine; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.200400295