3-sec-Butylpyridine

Base Information

Chemical Name:3-sec-Butylpyridine
CAS No.:25224-14-0
Molecular Formula:C₉H₁₃N
Molecular Weight:135.209
Hs Code.:
DSSTox Substance ID:DTXSID60865192
Nikkaji Number:J422.157E
Mol file:25224-14-0.mol

Synonyms:3-sec-Butylpyridine;25224-14-0;Pyridine, 3-(1-methylpropyl)-;3-(1-Methylpropyl)pyridine;SCHEMBL1245510;SCHEMBL22113733;DTXSID60865192

Suppliers and Price of 3-sec-Butylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-sec-Butylpyridine

Chemical Property:

Vapor Pressure:0.509mmHg at 25°C
Boiling Point:198.4°Cat760mmHg
PKA:5.61±0.11(Predicted)
Flash Point:66.8°C
PSA：12.89000
Density:0.906g/cm³
LogP:2.59510
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:135.104799419
Heavy Atom Count:10
Complexity:90.7

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(C)C1=CN=CC=C1

Technology Process of 3-sec-Butylpyridine

There total 8 articles about 3-sec-Butylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 110-89-4
piperidine

: 78-93-3
butanone

: 25224-14-0
3-(2'-butyl)pyridine

Guidance literature:: aluminum oxide; In benzene; at 420 ℃; in a flow-type glass reactor;

Reference yield:

: 626-60-8
3-Chloropyridine

: 15366-08-2,79722-38-6
s-butylmagnesium chloride

: 25224-14-0
3-(2'-butyl)pyridine

Guidance literature:: With 1-methyl-pyrrolidin-2-one; iron(III)-acetylacetonate; In tetrahydrofuran; at -20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/adsc.201601097

Reference yield:

: 78156-22-6
(+)-(S)-1,1-Diethoxy-3-sec-butyl-3-butene

: 25224-14-0
3-(2'-butyl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, Et₃N, RhCl(CO)(PPh₃)2 / 36 h / 80 - 100 °C / 76000 Torr

2: NH₂OH*HCl / ethanol; H₂O / 12 h / Heating

With chlorocarbonylbis(triphenylphosphine)rhodium(I); hydroxylamine hydrochloride; hydrogen; triethylamine; In ethanol; water;