[(4-Nitrophenyl)methylidene]propanedial

Base Information

• Chemical Name: [(4-Nitrophenyl)methylidene]propanedial
• CAS No.: 82700-48-9
• Molecular Formula: C₁₀H₇NO₄
• Molecular Weight: 205.17
• DSSTox Substance ID: DTXSID50512724
• Mol file: 82700-48-9.mol

Synonyms:82700-48-9;[(4-Nitrophenyl)methylidene]propanedial;DTXSID50512724

Chemical Property of [(4-Nitrophenyl)methylidene]propanedial

Chemical Property:

• XLogP3: 1.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 205.03750770
• Heavy Atom Count: 15
• Complexity: 274

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C=C(C=O)C=O)[N+](=O)[O-]

Technology Process of [(4-Nitrophenyl)methylidene]propanedial

There total 1 articles about [(4-Nitrophenyl)methylidene]propanedial which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

4-nitrobenzaldehdye (555-16-8) + 1,3-bis-dimethylaminotrimethinium perchlorate (1611-78-5) → p-Nitrobenzylidenemalonodialdehyde (82700-48-9)

Guidance literature:

With perchloric acid; In acetic anhydride; for 48h; Ambient temperature;

DOI:10.1016/S0040-4039(00)87200-7

Reference yield: 92.0%

tributylphosphine (998-40-3) + p-Nitrobenzylidenemalonodialdehyde (82700-48-9) → C22H34NO4P (118000-01-4)

Guidance literature:

In dichloromethane;

Reference yield: 62.0%

p-Nitrobenzylidenemalonodialdehyde (82700-48-9) + NCNMe2 (1467-79-4) → 2-Dimethylamino-4-(4-nitro-phenyl)-4H-[1,3]oxazine-5-carbaldehyde (104409-67-8)

Guidance literature:

In benzene; for 1h; Heating;

upstream raw materials:

4-nitrobenzaldehdye

1,3-bis-dimethylaminotrimethinium perchlorate

Downstream raw materials:

C₂₂H₃₄NO₄P

2-Dimethylamino-4-(4-nitro-phenyl)-4H-[1,3]oxazine-5-carbaldehyde

[(E)-2-Formyl-3-methoxy-1-(4-nitro-phenyl)-allyl]-phosphonic acid dimethyl ester

4-(4-Nitro-phenyl)-1,1-dioxo-5,7a-dihydro-1H-7-oxa-1λ⁶-thia-2,5-diaza-inden-6-one