Benzene, 1-(1-heptynylsulfonyl)-4-methyl-

Base Information

Chemical Name:Benzene, 1-(1-heptynylsulfonyl)-4-methyl-
CAS No.:82721-81-1
Molecular Formula:C14H18O2S
Molecular Weight:250.362
Hs Code.:
DSSTox Substance ID:DTXSID40458041
Nikkaji Number:J1.426.670D
Wikidata:Q82281165

Synonyms:Benzene, 1-(1-heptynylsulfonyl)-4-methyl-;1-Tosyl-1-heptyne;82721-81-1;DTXSID40458041

Suppliers and Price of Benzene, 1-(1-heptynylsulfonyl)-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzene, 1-(1-heptynylsulfonyl)-4-methyl-

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:250.10275099
Heavy Atom Count:17
Complexity:369

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCC#CS(=O)(=O)C1=CC=C(C=C1)C

Technology Process of Benzene, 1-(1-heptynylsulfonyl)-4-methyl-

There total 6 articles about Benzene, 1-(1-heptynylsulfonyl)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 82721-77-5
(E)-2-(phenylseleno)-1-(p-toluenesulfonyl)heptene

: 82721-81-1
1-(p-toluenesulfonyl)-1-heptyne

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; Ambient temperature;
DOI:10.1039/c39820000438

Reference yield:

: 628-71-7
1-Heptyne

: 824-79-3
sodium 4-methylbenzenesulfinate

: 82721-81-1
1-(p-toluenesulfonyl)-1-heptyne

Guidance literature:: With iodine; In ethyl acetate;
DOI:10.1016/S0040-4039(98)02441-1

Reference yield:

: 628-71-7
1-Heptyne

: 82721-81-1
1-(p-toluenesulfonyl)-1-heptyne

Guidance literature:: Multi-step reaction with 2 steps

1.1: CHCl₃ / 1 h / Irradiation

2.1: m-CPBA / CHCl₃ / 0.17 h / 20 °C

2.2: CHCl₃ / 1 h / Heating

With 3-chloro-benzenecarboperoxoic acid; In chloroform; 1.1: Addition / 2.1: Oxidation / 2.2: Elimination;
DOI:10.1021/jo000080p