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824-79-3

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Sodium toluene-4-sulphinate Manufacturer/High quality/Best price/In stock
Cas No: 824-79-3
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
China factory Sodium toluene-4-sulphinate CAS 824-79-3 99% Professional production
Cas No: 824-79-3
No Data 1 Metric Ton 1000 Kilogram/Month SHANXI JINJIN CHEMICAL INDUSTRIAL CO.,LTD Contact Supplier
Sodium p-tolylsulfinate
Cas No: 824-79-3
No Data No Data No Data Hangzhou Deli Chemical Co.,Ltd. Contact Supplier
High quality P-Toluene Sulfinic Acid Sodium Salt supplier in China
Cas No: 824-79-3
No Data 1 Metric Ton 30 Metric Ton/Month Simagchem Corporation Contact Supplier
Sodium toluene-4-sulphinate CAS NO.824-79-3
Cas No: 824-79-3
USD $ 1.0-3.0 / Kilogram 1 Kilogram 10 Kilogram/Day Hebei yanxi chemical co.,LTD. Contact Supplier
Sodium Toluene-4-Sulphinate (SPTS) CAS 824-79-3
Cas No: 824-79-3
No Data 1 Metric Ton Metric Ton/Day Hefei TNJ chemical industry co.,ltd Contact Supplier
SodiuM p-Toluenesulfinate
Cas No: 824-79-3
No Data 1 Kilogram 20 Metric Ton/Week Henan Allgreen Chemical Co.,Ltd Contact Supplier
Sodium p-toluenesulfinate
Cas No: 824-79-3
USD $ 2.0-3.0 / Kilogram 1 Kilogram 50 Metric Ton/Day EAST CHEMSOURCES LIMITED Contact Supplier
sodium 4-methylbenzenesulfinic acid
Cas No: 824-79-3
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
4-Toluenesulfinic acid sodium salt
Cas No: 824-79-3
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier

824-79-3 Usage

Chemical Properties

White powder

Uses

It can be used as intermediate of pharmaceutical and dispersal dyes, and also can be used as curing agent of grouting material.

Purification Methods

Recrystallise the salt from water (to constant UV spectrum) and dry it under vacuum, or extract it with hot *benzene, then dissolve it in EtOH/H2O and heat with decolorising charcoal. The solution is filtered and cooled to give crystals of the dihydrate.[Beilstein 11 I 718.]
InChI:InChI=1/C7H7O2S.Na/c1-6-2-4-7(5-3-6)10(8)9;/h2-5H,1H3;/rC7H7NaO2S/c1-6-2-4-7(5-3-6)11(8,9)10/h2-5H,1H3

824-79-3 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Sigma-Aldrich (89720)  Sodiump-toluenesulfinate  purum, anhydrous, ≥96.0% (NT) 824-79-3 89720-500G 5,496.66CNY Detail
Sigma-Aldrich (89720)  Sodiump-toluenesulfinate  purum, anhydrous, ≥96.0% (NT) 824-79-3 89720-100G 1,409.85CNY Detail
Aldrich (455652)  Sodiump-toluenesulfinate  95% 824-79-3 455652-100G 909.09CNY Detail
Aldrich (455652)  Sodiump-toluenesulfinate  95% 824-79-3 455652-25G 308.88CNY Detail
Alfa Aesar (A11430)  p-Toluenesulfinic acid sodium salt, 97% (dry wt.), water <5%    824-79-3 500g 1051.0CNY Detail
Alfa Aesar (A11430)  p-Toluenesulfinic acid sodium salt, 97% (dry wt.), water <5%    824-79-3 100g 448.0CNY Detail
Alfa Aesar (A11430)  p-Toluenesulfinic acid sodium salt, 97% (dry wt.), water <5%    824-79-3 25g 223.0CNY Detail

824-79-3SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Sodium p-Toluenesulfinate

1.2 Other means of identification

Product number -
Other names sodium,4-methylbenzenesulfinate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:824-79-3 SDS

824-79-3Synthetic route

di(4-methyl)phenylthiosulfonate
2943-42-2

di(4-methyl)phenylthiosulfonate

copper(I) cyanide
544-92-3

copper(I) cyanide

A

4-tolyl thiocyanate
5285-74-5

4-tolyl thiocyanate

B

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

Conditions
ConditionsYield
In acetonitrile at 100℃; for 12h;A 93%
B 100%
p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

Conditions
ConditionsYield
With hydrazine hydrate; sodium carbonate In water at 80℃; for 2h;97.8%
With sodium carbonate; sodium sulfite In water at 52℃; pH=7.2; Temperature;96.9%
With sodium hydrogencarbonate; sodium sulfite In water at 70 - 80℃; for 1h;96%
p-toluene sulfinic acid
536-57-2

p-toluene sulfinic acid

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 40℃; for 2h;96.6%
formaldehyd
50-00-0

formaldehyd

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

Conditions
ConditionsYield
Stage #1: p-toluenesulfonyl chloride With sodium hydrogencarbonate; sodium sulfite In water at 70 - 80℃; for 1h;
Stage #2: formaldehyd at 90℃;
96%
C29H33N3O3S

C29H33N3O3S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-Cyclohexyl-4-(4-methoxy-phenyl)-6-phenyl-1,6-dihydro-[1,2,3]triazine

1-Cyclohexyl-4-(4-methoxy-phenyl)-6-phenyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 95%
toluene
108-88-3

toluene

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

Conditions
ConditionsYield
Stage #1: toluene With aluminum (III) chloride; 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate In dichloromethane at 0℃; for 2h;
Stage #2: With sodium hydrogencarbonate In dichloromethane; water at 0℃;
95%
With aluminum (III) chloride; 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate; sodium hydrogencarbonate In dichloromethane; water at 20 - 30℃;83%
C28H30N4O4S

C28H30N4O4S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-Cyclohexyl-6-(4-nitro-phenyl)-4-phenyl-1,6-dihydro-[1,2,3]triazine

1-Cyclohexyl-6-(4-nitro-phenyl)-4-phenyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 93%
C28H31N3O2S

C28H31N3O2S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-Cyclohexyl-4,6-diphenyl-1,6-dihydro-[1,2,3]triazine

1-Cyclohexyl-4,6-diphenyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 92%
C29H27N3O2S

C29H27N3O2S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-Benzyl-4,6-diphenyl-1,6-dihydro-[1,2,3]triazine

1-Benzyl-4,6-diphenyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 91%
N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-S-methyl-S-(4-methylphenyl)sulfoximide
1192657-22-9

N-(9,10-dioxo-9,10-dihydroanthracen-1-yl)-S-methyl-S-(4-methylphenyl)sulfoximide

A

2,6-dihydronaphtho[1,2,3-cd]indol-6-one
42326-31-8

2,6-dihydronaphtho[1,2,3-cd]indol-6-one

B

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

Conditions
ConditionsYield
With sodium methylate In tetrahydrofuran for 0.333333h; Reflux;A 91%
B 76%
C29H33N3O2S

C29H33N3O2S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-Cyclohexyl-4-phenyl-6-p-tolyl-1,6-dihydro-[1,2,3]triazine

1-Cyclohexyl-4-phenyl-6-p-tolyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 90%
C28H30ClN3O2S

C28H30ClN3O2S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

4-(4-Chloro-phenyl)-1-cyclohexyl-6-phenyl-1,6-dihydro-[1,2,3]triazine

4-(4-Chloro-phenyl)-1-cyclohexyl-6-phenyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 90%
C29H33N3O3S

C29H33N3O3S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-Cyclohexyl-6-(4-methoxy-phenyl)-4-phenyl-1,6-dihydro-[1,2,3]triazine

1-Cyclohexyl-6-(4-methoxy-phenyl)-4-phenyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 90%
C25H27N3O2S

C25H27N3O2S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-Isopropyl-4,6-diphenyl-1,6-dihydro-[1,2,3]triazine

1-Isopropyl-4,6-diphenyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 89%
With sodium hydride In 1,2-dimethoxyethane Product distribution; Mechanism; 5 h, room t. then 15 min, reflux; reactions of derivatives;A n/a
B 89%
6,7-dihydro-5,7-dimethyl-3-phenyl-1-tosyl-1,2-diazepine
93627-03-3

6,7-dihydro-5,7-dimethyl-3-phenyl-1-tosyl-1,2-diazepine

A

3,5-dimethyl-7-phenyl-3H-1,2-diazepine
93627-06-6

3,5-dimethyl-7-phenyl-3H-1,2-diazepine

B

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

Conditions
ConditionsYield
With sodium ethanolate In toluene for 0.0833333h;A 84%
B n/a
C28H30N4O4S

C28H30N4O4S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-Cyclohexyl-4-(4-nitro-phenyl)-6-phenyl-1,6-dihydro-[1,2,3]triazine

1-Cyclohexyl-4-(4-nitro-phenyl)-6-phenyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 83%
C29H33N3O2S

C29H33N3O2S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-Cyclohexyl-6-phenyl-4-p-tolyl-1,6-dihydro-[1,2,3]triazine

1-Cyclohexyl-6-phenyl-4-p-tolyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 82%
sodium salt of α-(cyclopenten-1-yl)acetophenone N-tosylhydrazone
73594-32-8

sodium salt of α-(cyclopenten-1-yl)acetophenone N-tosylhydrazone

A

2-Phenyl-3b,4,5,6-tetrahydro-1H-3,3a-diaza-cyclopropadicyclopentene
73594-35-1

2-Phenyl-3b,4,5,6-tetrahydro-1H-3,3a-diaza-cyclopropadicyclopentene

B

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

Conditions
ConditionsYield
In tetrachloromethane for 2h; Heating;A 73%
B n/a
sodium salt of (Z)-(p-bromophenyl)-4-methyl-3-hexen-1-one N-tosylhydrazone
100189-03-5

sodium salt of (Z)-(p-bromophenyl)-4-methyl-3-hexen-1-one N-tosylhydrazone

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

3-(p-bromophenyl)-6-endo-ethyl-6-exo-methyl-1,2-diazabicyclo<3.1.0>hex-2-ene
100189-09-1

3-(p-bromophenyl)-6-endo-ethyl-6-exo-methyl-1,2-diazabicyclo<3.1.0>hex-2-ene

Conditions
ConditionsYield
In tetrachloromethane Heating;A n/a
B 70%
sodium salt of (E)-1,6-diphenyl-5-hexen-1-one N-tosylhydrazone
100188-83-8

sodium salt of (E)-1,6-diphenyl-5-hexen-1-one N-tosylhydrazone

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

(3aS,6aS)-3,6a-Diphenyl-3,3a,4,5,6,6a-hexahydro-cyclopentapyrazole
87013-65-8

(3aS,6aS)-3,6a-Diphenyl-3,3a,4,5,6,6a-hexahydro-cyclopentapyrazole

Conditions
ConditionsYield
In tetrachloromethane for 1h; Heating;A n/a
B 69%
sodium salt of 1-(p-chlorophenyl)-4-methyl-3-penten-1-one N-tosylhydrazone
100189-05-7

sodium salt of 1-(p-chlorophenyl)-4-methyl-3-penten-1-one N-tosylhydrazone

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

3-(p-chlorophenyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene
87013-68-1

3-(p-chlorophenyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene

Conditions
ConditionsYield
In tetrachloromethane Heating;A n/a
B 68%
sodium salt of (Z)-1-phenyl-3-penten-1-one N-tosylhydrazone
100189-02-4

sodium salt of (Z)-1-phenyl-3-penten-1-one N-tosylhydrazone

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

3-phenyl-6-endo-ethyl-6-exo-methyl-1,2-diazabicyclo<3.1.0>hex-2-ene
100189-08-0

3-phenyl-6-endo-ethyl-6-exo-methyl-1,2-diazabicyclo<3.1.0>hex-2-ene

Conditions
ConditionsYield
In tetrachloromethane Heating;A n/a
B 65%
sodium salt of 1-(p-bromophenyl)-4-methyl-3-penten-1-one N-tosylhydrazone
100189-04-6

sodium salt of 1-(p-bromophenyl)-4-methyl-3-penten-1-one N-tosylhydrazone

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

3-(p-bromophenyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene
87013-67-0

3-(p-bromophenyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene

Conditions
ConditionsYield
In tetrachloromethane Heating;A n/a
B 65%
C26H29N3O2S

C26H29N3O2S

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

1-tert-Butyl-4,6-diphenyl-1,6-dihydro-[1,2,3]triazine

1-tert-Butyl-4,6-diphenyl-1,6-dihydro-[1,2,3]triazine

Conditions
ConditionsYield
With sodium hydride In monoethylene glycol diethyl ether 5 h, room t. then 15 min, reflux;A n/a
B 65%
sodium salt of 1-(p-anisyl)-4-methyl-3-penten-1-one N-tosylhydrazone
100189-07-9

sodium salt of 1-(p-anisyl)-4-methyl-3-penten-1-one N-tosylhydrazone

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

3-(p-anisyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene
87013-70-5

3-(p-anisyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene

Conditions
ConditionsYield
In tetrachloromethane Heating;A n/a
B 62%
sodium salt of 1-(p-cyanophenyl)-4-methyl-3-penten-1-one N-tosylhydrazone
100189-12-6

sodium salt of 1-(p-cyanophenyl)-4-methyl-3-penten-1-one N-tosylhydrazone

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

3-(p-cyanophenyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene
100189-14-8

3-(p-cyanophenyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene

Conditions
ConditionsYield
In tetrachloromethane Heating;A n/a
B 61%
sodium salt of 1-(m-nitrophenyl)-4-methyl-3-penten-1-one N-tosylhydrazone
100189-11-5

sodium salt of 1-(m-nitrophenyl)-4-methyl-3-penten-1-one N-tosylhydrazone

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

3-(m-nitrophenyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene
100189-13-7

3-(m-nitrophenyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene

Conditions
ConditionsYield
In tetrachloromethane Heating;A n/a
B 61%
p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

A

di(p-tolyl) disulfide
103-19-5

di(p-tolyl) disulfide

B

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

Conditions
ConditionsYield
With sodium p-thiocresolate In ethanol at 50℃; for 0.833333h;A n/a
B 61%
sodium salt of 1-(p-tolyl)-4-methyl-3-penten-1-one N-tosylhydrazone
100189-06-8

sodium salt of 1-(p-tolyl)-4-methyl-3-penten-1-one N-tosylhydrazone

A

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

B

3-(p-tolyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene
87013-69-2

3-(p-tolyl)-6,6-dimethyl-1,2-diazabicyclo<3.1.0>hex-2-ene

Conditions
ConditionsYield
In tetrachloromethane Heating;A n/a
B 60%
trans-geranyl bromide
6138-90-5

trans-geranyl bromide

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

3,7-dimethyl-1-(p-toluenesulfonyl)-2(E),6-octadiene
53254-60-7

3,7-dimethyl-1-(p-toluenesulfonyl)-2(E),6-octadiene

Conditions
ConditionsYield
With carbon tetrabromide; tetra-(n-butyl)ammonium iodide In tetrahydrofuran at 20℃; for 24h;100%
In N,N-dimethyl-formamide for 24h; Ambient temperature;96%
In N,N-dimethyl-formamide72%
pyrrolidine
123-75-1

pyrrolidine

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

N-tosylpyrrolidine
6435-78-5

N-tosylpyrrolidine

Conditions
ConditionsYield
With sodium hypochlorite In water Ambient temperature;100%
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide In water; acetonitrile at 50℃; for 8h;95%
With ammonium bromide In water; acetonitrile Electrolysis;95%
2-(bromomethyl)-6-methyl-4H-pyran-4-one
99809-37-7

2-(bromomethyl)-6-methyl-4H-pyran-4-one

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

2-methyl-6-<(p-tolylsulfonylfonyl)methyl>-4H-pyran-4-one
99809-38-8

2-methyl-6-<(p-tolylsulfonylfonyl)methyl>-4H-pyran-4-one

Conditions
ConditionsYield
In ethanol for 1h; Heating;100%
1-hexene
592-41-6

1-hexene

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

2-iodo-1-tosylhexane
71963-96-7

2-iodo-1-tosylhexane

Conditions
ConditionsYield
With iodine In water; ethyl acetate at 20℃; for 1.33333h; iodosulfonization;100%
With iodine In water; ethyl acetate for 2h; Ambient temperature;
dimethylchloroamine
1585-74-6

dimethylchloroamine

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

N,N,4-trimethylbenzenesulfonamide
599-69-9

N,N,4-trimethylbenzenesulfonamide

Conditions
ConditionsYield
In water Ambient temperature;100%
1-penten
109-67-1

1-penten

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

1-(2-Iodo-pentane-1-sulfonyl)-4-methyl-benzene

1-(2-Iodo-pentane-1-sulfonyl)-4-methyl-benzene

Conditions
ConditionsYield
With iodine In water; ethyl acetate at 20℃; for 1.33333h; iodosulfonization;100%
With iodine In water; ethyl acetate for 2h; Ambient temperature;
1-undecene
821-95-4

1-undecene

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

1-(2-Iodo-undecane-1-sulfonyl)-4-methyl-benzene

1-(2-Iodo-undecane-1-sulfonyl)-4-methyl-benzene

Conditions
ConditionsYield
With iodine In water; ethyl acetate at 20℃; for 1.33333h; iodosulfonization;100%
With iodine In water; ethyl acetate for 2h; Ambient temperature;
2-chloro-2-methyl-3-(p-nitrophenyl)-3-propanone
83846-29-1

2-chloro-2-methyl-3-(p-nitrophenyl)-3-propanone

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

α-(p-methylbenzenesulfonyl)-p-nitroisobutyrophenone

α-(p-methylbenzenesulfonyl)-p-nitroisobutyrophenone

Conditions
ConditionsYield
With potassium tert-butylate In dimethyl sulfoxide for 6.5h; Irradiation;100%
sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

sodium 4-methylbenzenesulfonothioate
3753-27-3

sodium 4-methylbenzenesulfonothioate

Conditions
ConditionsYield
With sulfur; N-butylamine at 20℃; for 0.5h; Other amines. In a titanium autoclave.;100%
With sulfur In pyridine for 48h; Ambient temperature;92%
With pyridine; sulfur at 20℃; for 16h;92%
benzyl bromide
100-39-0

benzyl bromide

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

1-methyl-4-(benzylsulfonyl)benzene
5395-20-0

1-methyl-4-(benzylsulfonyl)benzene

Conditions
ConditionsYield
In 1,4-dioxane; water100%
With 1-butyl-3-methylimidazolium Tetrafluoroborate In water at 60℃; for 1h;96%
With polyethylene polyamine functionalized polyacrylonitrile fiber In water at 90℃; for 0.5h; Reagent/catalyst; Green chemistry;95%
sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

buta-1,3-diene
106-99-0

buta-1,3-diene

(E)-1-iodo-4-tosyl-2-butene
115147-52-9

(E)-1-iodo-4-tosyl-2-butene

Conditions
ConditionsYield
With iodine In water; ethyl acetate at 20℃; for 3h; iodosulfonization;100%
With iodine In dichloromethane for 6h; Ambient temperature;93%
sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

α-bromoacetophenone
70-11-1

α-bromoacetophenone

1-phenyl-2-tosylethanone
31378-03-7

1-phenyl-2-tosylethanone

Conditions
ConditionsYield
In 1,4-dioxane Reflux;100%
In 1,4-dioxane; water Reflux;100%
In 1,4-dioxane; water Inert atmosphere;100%
sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

1-amino-2-propene
107-11-9

1-amino-2-propene

4-methyl-N-(2-propenyl)benzenesulfonamide
50487-71-3

4-methyl-N-(2-propenyl)benzenesulfonamide

Conditions
ConditionsYield
With sodium hypochlorite In water Ambient temperature;100%
With iodine In water at 20℃; for 3h; Green chemistry;81%
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide In water; acetonitrile at 50℃; for 8h;80%
methanol
67-56-1

methanol

α-methoxystyrene
4747-13-1

α-methoxystyrene

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

1-phenyl-2-(p-tolylsulfonyl)ethanone dimethyl acetal
86409-96-3

1-phenyl-2-(p-tolylsulfonyl)ethanone dimethyl acetal

Conditions
ConditionsYield
With tris(pyridine-2-carboxylato)manganese(III) at 0℃;100%
4-Nitrophenacyl bromide
99-81-0

4-Nitrophenacyl bromide

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

1-(4-nitrophenyl)-2-(toluene-4-sulfonyl)ethanone
56858-46-9

1-(4-nitrophenyl)-2-(toluene-4-sulfonyl)ethanone

Conditions
ConditionsYield
In 1,4-dioxane; water Reflux;100%
In ethanol Heating;
In ethanol; water at 100℃; for 0.166667h; microwave irradiation;
sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

2-Bromo-4'-methoxyacetophenone
2632-13-5

2-Bromo-4'-methoxyacetophenone

1-(4-methoxyphenyl)-2-tosylethanone
86516-51-0

1-(4-methoxyphenyl)-2-tosylethanone

Conditions
ConditionsYield
In 1,4-dioxane; water Reflux;100%
In ethanol for 1.5h; Heating;90%
In ethanol Heating;
sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

p-toluene sulfinic acid
536-57-2

p-toluene sulfinic acid

Conditions
ConditionsYield
With hydrogenchloride In tert-butyl methyl ether; water for 0.166667h;100%
With hydrogenchloride In tert-butyl methyl ether; water for 0.166667h;100%
With hydrogenchloride In tert-butyl methyl ether; water Inert atmosphere; Schlenk technique;97%
homoalylic alcohol
627-27-0

homoalylic alcohol

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

3-Iodo-4-(toluene-4-sulfonyl)-butan-1-ol

3-Iodo-4-(toluene-4-sulfonyl)-butan-1-ol

Conditions
ConditionsYield
With iodine In water; ethyl acetate at 20℃; for 2.5h; iodosulfonization;100%
1-dodecene
112-41-4

1-dodecene

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

1-(2-iodo-dodecane-1-sulfonyl)-4-methyl-benzene

1-(2-iodo-dodecane-1-sulfonyl)-4-methyl-benzene

Conditions
ConditionsYield
With iodine In water; ethyl acetate at 20℃; for 1.33333h; iodosulfonization;100%
Dimethyldisulphide
624-92-0

Dimethyldisulphide

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

methyl thiotosylate
4973-66-4

methyl thiotosylate

Conditions
ConditionsYield
With iodine In dichloromethane at 20℃; for 1h;100%
With iodine at 30℃; for 2h;90%
With copper(l) iodide; 1,10-Phenanthroline; ammonium tetrafluoroborate In N,N-dimethyl acetamide; water at 30℃; for 36h;79%
bromoacetic acid tert-butyl ester
5292-43-3

bromoacetic acid tert-butyl ester

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

tert-butyl [(4-methylphenyl)sulfonyl]acetate
98317-43-2

tert-butyl [(4-methylphenyl)sulfonyl]acetate

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 24h;100%
In 1,4-dioxane; water for 10h; Heating;
sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

4-(bromoacetyl)toluene
619-41-0

4-(bromoacetyl)toluene

2-(toluene-4-sulfonyl)-1-p-tolylethanone
61820-95-9

2-(toluene-4-sulfonyl)-1-p-tolylethanone

Conditions
ConditionsYield
In 1,4-dioxane; water Reflux;100%
With PEG-400 at 20℃; for 0.166667h;90%
In 1,4-dioxane; water for 6h; Reflux; Inert atmosphere;
In ethanol for 6h; Reflux;
In tetrahydrofuran; dimethyl sulfoxide at 20℃; for 0.75h; Green chemistry;170 mg
2-Fluorobenzaldehyde
446-52-6

2-Fluorobenzaldehyde

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

2-(toluene-4-sulfonyl)benzaldehyde

2-(toluene-4-sulfonyl)benzaldehyde

Conditions
ConditionsYield
In dimethyl sulfoxide at 150℃; for 15h;100%
In dimethyl sulfoxide at 100℃; for 16h;39%
sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

cyclohexene
110-83-8

cyclohexene

1-((2-iodocyclohexyl)sulfonyl)-4-methylbenzene
501652-27-3

1-((2-iodocyclohexyl)sulfonyl)-4-methylbenzene

Conditions
ConditionsYield
With iodine In dichloromethane; water at 20℃;100%
With potassium iodide In acetonitrile at 20℃; for 1h;
sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

2-Bromo-4'-phenylacetophenone
135-73-9

2-Bromo-4'-phenylacetophenone

1-[1,1'-biphenyl]-4-yl-2-[(4-methylphenyl)sulfonyl]-1-ethanone
710984-37-5

1-[1,1'-biphenyl]-4-yl-2-[(4-methylphenyl)sulfonyl]-1-ethanone

Conditions
ConditionsYield
In 1,4-dioxane; water Reflux;100%
In 1,4-dioxane; water for 6h; Inert atmosphere; Reflux;
In 1,4-dioxane; water for 6h; Reflux; Inert atmosphere;
In ethanol; water Reflux;
N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)phenoxyacetamide
1413925-82-2

N-(2,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)phenoxyacetamide

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

N-[4-hydroxy-2,5-dimethyl-3-(4-methylbenzenesulfonyl)phenyl]-2-phenoxyacetamide

N-[4-hydroxy-2,5-dimethyl-3-(4-methylbenzenesulfonyl)phenyl]-2-phenoxyacetamide

Conditions
ConditionsYield
In acetic acid at 20℃;100%
N-(2,6-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)phenoxyacetamide
1413925-83-3

N-(2,6-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)phenoxyacetamide

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

N-(4-hydroxy-2,6-dimethylphenyl)-N-(4-methylbenzenesulfonyl)-2-phenoxyacetamide

N-(4-hydroxy-2,6-dimethylphenyl)-N-(4-methylbenzenesulfonyl)-2-phenoxyacetamide

Conditions
ConditionsYield
In acetic acid at 20℃;100%
N-(3,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)phenoxyacetamide
1413925-85-5

N-(3,5-dimethyl-4-oxocyclohexa-2,5-dien-1-ylidene)phenoxyacetamide

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

2,6-dimethyl-4-(2-phenoxyacetylamino)phenyl 4-methylbenzenesulfonate

2,6-dimethyl-4-(2-phenoxyacetylamino)phenyl 4-methylbenzenesulfonate

Conditions
ConditionsYield
In acetic acid at 20℃;100%
1,2,4-tris-(3-chloro-3-thia-propyl)cyclohexane
1225201-62-6

1,2,4-tris-(3-chloro-3-thia-propyl)cyclohexane

sodium 4-methylbenzenesulfinate
824-79-3

sodium 4-methylbenzenesulfinate

toluene-4-thiosulfonic acid S-{2-[2,4-bis(2-toluene-4-sulfonylsulfanylethyl)cyclohexyl]ethyl} ester

toluene-4-thiosulfonic acid S-{2-[2,4-bis(2-toluene-4-sulfonylsulfanylethyl)cyclohexyl]ethyl} ester

Conditions
ConditionsYield
In tetrachloromethane at 26℃;100%

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