Phosphine, dicyclohexyl[3-(phenylphosphino)propyl]-

Base Information

Chemical Name:Phosphine, dicyclohexyl[3-(phenylphosphino)propyl]-
CAS No.:82763-84-6
Molecular Formula:C21H34P2
Molecular Weight:348.448
Hs Code.:
DSSTox Substance ID:DTXSID80423213
Wikidata:Q82235367

Synonyms:Phosphine, dicyclohexyl[3-(phenylphosphino)propyl]-;82763-84-6;DTXSID80423213

Suppliers and Price of Phosphine, dicyclohexyl[3-(phenylphosphino)propyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Phosphine, dicyclohexyl[3-(phenylphosphino)propyl]-

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:7
Exact Mass:348.21357508
Heavy Atom Count:23
Complexity:281

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)P(CCCPC2=CC=CC=C2)C3CCCCC3

Technology Process of Phosphine, dicyclohexyl[3-(phenylphosphino)propyl]-

There total 2 articles about Phosphine, dicyclohexyl[3-(phenylphosphino)propyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 71734-57-1
1-chloro-3-(dicyclohexylphosphino)propane

: 638-21-1
phenylphosphane

: 82763-84-6
(+/-)-1-(dicyclohexylphosphino)-3-(phenylphosphino)propane

Guidance literature:: With sodium; In diethyl ether; ammonia; toluene; at -78 ℃;
DOI:10.1021/ja00333a036

Reference yield:

: 829-84-5
dicyclohexylphosphane

: 82763-84-6
(+/-)-1-(dicyclohexylphosphino)-3-(phenylphosphino)propane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1.2 M methyllithium / 1.) tetrahydrofuran, diethyl ether, 0 deg C; 2.) diethyl ether, r.t.

2: 65 percent / sodium / toluene; liquid ammonia; diethyl ether / -78 °C

With methyllithium; sodium; In diethyl ether; ammonia; toluene;
DOI:10.1021/ja00333a036

Reference yield: 86.0%

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 82763-84-6
(+/-)-1-(dicyclohexylphosphino)-3-(phenylphosphino)propane

: 88496-14-4
PtCl₂((C₆H₅)2PCH₂CH₂CH₂P(Ph)H)

Guidance literature:: In toluene; benzene; under N2 atm. slurry PtCl2(COD) in benzene treated with toluene soln. cyppH; mixt. filtered, filtrate reduced in stream N2, Et2O added, product filtered; washed with Et2O and recrystd. from CH3NO2; elem. anal.;