Indan-1-one (2,4-dinitrophenyl)hydrazone

Base Information

Chemical Name:Indan-1-one (2,4-dinitrophenyl)hydrazone
CAS No.:902-25-0
Molecular Formula:C15H12N4O4
Molecular Weight:312.285
Hs Code.:
NSC Number:61654
Nikkaji Number:J2.348.248G

Synonyms:Indan-1-one (2,4-dinitrophenyl)hydrazone;902-25-0;N-[(Z)-2,3-dihydroinden-1-ylideneamino]-2,4-dinitroaniline;NSC61654;NSC-61654;Z49555080

Suppliers and Price of Indan-1-one (2,4-dinitrophenyl)hydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Indan-1-one (2,4-dinitrophenyl)hydrazone

Chemical Property:

Vapor Pressure:6.36E-10mmHg at 25°C
Boiling Point:494.6°Cat760mmHg
Flash Point:252.9°C
Density:1.49g/cm³
XLogP3:4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:312.08585488
Heavy Atom Count:23
Complexity:499

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=NNC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])C3=CC=CC=C31
Isomeric SMILES:C1C/C(=N/NC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])/C3=CC=CC=C31

Technology Process of Indan-1-one (2,4-dinitrophenyl)hydrazone

There total 5 articles about Indan-1-one (2,4-dinitrophenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 6351-10-6
1-Indanol

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 902-25-0
1-indanone 2,4-dinitrophenylhydrazone

Guidance literature:: 1-Indanol; With peracetic acid; C₉H₁₇NO₅S^(1-)*C₁₂H₁₁IN⁽¹⁺⁾; acetic acid; In 1,1,1,3',3',3'-hexafluoro-propanol; at 20 ℃; for 12h;

(2,4-dinitro-phenyl)-hydrazine; With sulfuric acid; In diethyl ether; ethanol; water;
DOI:10.1016/j.tetlet.2012.01.053

Reference yield:

: 83-33-0
inden-1-one

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 902-25-0
1-indanone 2,4-dinitrophenylhydrazone

Guidance literature:

Reference yield:

: 6351-10-6
1-Indanol

: 902-25-0
1-indanone 2,4-dinitrophenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: (diacetoxyiodo)benzene / RuCl₃ / acetonitrile; H₂O / 1.5 h / 20 °C

2: H₂SO₄ / acetonitrile; H₂O; ethanol

With [bis(acetoxy)iodo]benzene; sulfuric acid; ruthenium trichloride; In ethanol; water; acetonitrile;
DOI:10.1016/j.tetlet.2006.06.100