Technology Process of 2-Propenoic acid, 2-[(phenylthio)methyl]-, ethyl ester
There total 5 articles about 2-Propenoic acid, 2-[(phenylthio)methyl]-, ethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
2: triethylamine / ethanol / 20 °C / Inert atmosphere
3: ethanol / Reflux; Inert atmosphere
With
sodium hydride; triethylamine;
In
tetrahydrofuran; ethanol;
2: |Michael Addition;
DOI:10.1080/10426507.2021.1948850
- Guidance literature:
-
Multi-step reaction with 4 steps
1: phosphorus tribromide / diethyl ether / 3 h / -10 °C / Inert atmosphere
2: sodium hydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
3: triethylamine / ethanol / 20 °C / Inert atmosphere
4: ethanol / Reflux; Inert atmosphere
With
phosphorus tribromide; sodium hydride; triethylamine;
In
tetrahydrofuran; diethyl ether; ethanol;
3: |Michael Addition;
DOI:10.1080/10426507.2021.1948850
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / ethanol / 20 °C / Inert atmosphere
2: ethanol / Reflux; Inert atmosphere
With
triethylamine;
In
ethanol;
1: |Michael Addition;
DOI:10.1080/10426507.2021.1948850
