Acetonitrile, [(4-methylphenyl)nitrosoamino]-

Base Information

Chemical Name:Acetonitrile, [(4-methylphenyl)nitrosoamino]-
CAS No.:829-28-7
Molecular Formula:C9H9N3O
Molecular Weight:175.19
Hs Code.:
DSSTox Substance ID:DTXSID50400399
Wikidata:Q82203355

Synonyms:Acetonitrile, [(4-methylphenyl)nitrosoamino]-;829-28-7;DTXSID50400399;AKOS001063201;Z56855169

Suppliers and Price of Acetonitrile, [(4-methylphenyl)nitrosoamino]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Acetonitrile, [(4-methylphenyl)nitrosoamino]-

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:175.074561919
Heavy Atom Count:13
Complexity:212

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N(CC#N)N=O

Technology Process of Acetonitrile, [(4-methylphenyl)nitrosoamino]-

There total 3 articles about Acetonitrile, [(4-methylphenyl)nitrosoamino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: p-Tolylamino-acetonitrile; hydrochloride

: 829-28-7
N-Nitroso-N-(4-methyl-phenylamino)-acetonitril

Guidance literature:: With sodium nitrite; In water; for 17h; Ambient temperature;
DOI:10.1021/jo00234a018

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 829-28-7
N-Nitroso-N-(4-methyl-phenylamino)-acetonitril

Guidance literature:: Multi-step reaction with 2 steps

1: conc. HCl / methanol; H₂O / 3 h / 20 °C

2: 39 percent / NaNO₂ / H₂O / 17 h / Ambient temperature

With hydrogenchloride; sodium nitrite; In methanol; water;
DOI:10.1021/jo00234a018