1H-Pyrrole, 1-[(2-bromo-4,5-dimethoxyphenyl)sulfonyl]-2,5-dihydro-

Base Information

Chemical Name:1H-Pyrrole, 1-[(2-bromo-4,5-dimethoxyphenyl)sulfonyl]-2,5-dihydro-
CAS No.:830319-62-5
Molecular Formula:C12H14BrNO4S
Molecular Weight:348.217
Hs Code.:
DSSTox Substance ID:DTXSID40479897
Wikidata:Q82314236

Synonyms:830319-62-5;1H-Pyrrole, 1-[(2-bromo-4,5-dimethoxyphenyl)sulfonyl]-2,5-dihydro-;DTXSID40479897

Suppliers and Price of 1H-Pyrrole, 1-[(2-bromo-4,5-dimethoxyphenyl)sulfonyl]-2,5-dihydro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1H-Pyrrole, 1-[(2-bromo-4,5-dimethoxyphenyl)sulfonyl]-2,5-dihydro-

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:346.98269
Heavy Atom Count:19
Complexity:426

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=C(C=C1OC)Br)S(=O)(=O)N2CC=CC2

Technology Process of 1H-Pyrrole, 1-[(2-bromo-4,5-dimethoxyphenyl)sulfonyl]-2,5-dihydro-

There total 4 articles about 1H-Pyrrole, 1-[(2-bromo-4,5-dimethoxyphenyl)sulfonyl]-2,5-dihydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 109-96-6,760178-50-5
3-Pyrroline

: 51072-64-1
2-bromo-4,5-dimethoxybenzene-1-sulfonyl chloride

: 830319-62-5
1-(2-bromo-4,5-dimethoxybenzenesulfonyl)-2,5-dihydro-1H-pyrrole

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 15h;
DOI:10.1021/ol0480123

Reference yield: 83.0%

: 830319-61-4
N,N-diallyl-2-bromo-4,5-dimethoxybenzenesulfonamide

: 830319-62-5
1-(2-bromo-4,5-dimethoxybenzenesulfonyl)-2,5-dihydro-1H-pyrrole

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/ol0480123

Reference yield:

: 2859-78-1
4-Bromoveratrole

: 830319-62-5
1-(2-bromo-4,5-dimethoxybenzenesulfonyl)-2,5-dihydro-1H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / chlorosulfonic acid / 0.58 h / 0 °C

2: 93 percent / triethylamine / CH₂Cl₂ / 15 h / 0 - 20 °C

With chlorosulfonic acid; triethylamine; In dichloromethane;
DOI:10.1021/ol0480123