2-Thiophenesulfonyl chloride, 5-[2-[(4-chlorophenyl)amino]-2-oxoethyl]-

Base Information

Chemical Name:2-Thiophenesulfonyl chloride, 5-[2-[(4-chlorophenyl)amino]-2-oxoethyl]-
CAS No.:830330-70-6
Molecular Formula:C12H9Cl2NO3S2
Molecular Weight:350.246
Hs Code.:
DSSTox Substance ID:DTXSID20465617
Wikidata:Q82291730

Synonyms:830330-70-6;2-Thiophenesulfonyl chloride, 5-[2-[(4-chlorophenyl)amino]-2-oxoethyl]-;DTXSID20465617

Suppliers and Price of 2-Thiophenesulfonyl chloride, 5-[2-[(4-chlorophenyl)amino]-2-oxoethyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Thiophenesulfonyl chloride, 5-[2-[(4-chlorophenyl)amino]-2-oxoethyl]-

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:348.9400909
Heavy Atom Count:20
Complexity:444

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1NC(=O)CC2=CC=C(S2)S(=O)(=O)Cl)Cl

Technology Process of 2-Thiophenesulfonyl chloride, 5-[2-[(4-chlorophenyl)amino]-2-oxoethyl]-

There total 2 articles about 2-Thiophenesulfonyl chloride, 5-[2-[(4-chlorophenyl)amino]-2-oxoethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39098-97-0
2-thienylacetic acid chloride

: 830330-70-6
5-[(4-chlorophenylcarbamoyl)methyl]thiophene-2-sulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / iPr₂NEt / CH₂Cl₂ / 0 - 20 °C

2: 47 percent / ClSO₃H / CH₂Cl₂ / 5 h / -80 - 20 °C

With chlorosulfonic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm031112e

Reference yield:

: 106-47-8
4-chloro-aniline

: 830330-70-6
5-[(4-chlorophenylcarbamoyl)methyl]thiophene-2-sulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / iPr₂NEt / CH₂Cl₂ / 0 - 20 °C

2: 47 percent / ClSO₃H / CH₂Cl₂ / 5 h / -80 - 20 °C

With chlorosulfonic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm031112e