Technology Process of Benzo[b]thiophene-4-ol, 6-[(1E)-2-(3,4,5-trimethoxyphenyl)ethenyl]-,
acetate
There total 6 articles about Benzo[b]thiophene-4-ol, 6-[(1E)-2-(3,4,5-trimethoxyphenyl)ethenyl]-,
acetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
for 0.166667h;
DOI:10.1021/jm0510732
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 76 percent / imidazole / CH2Cl2 / 18 h / 20 °C
2: LiAlH4 / tetrahydrofuran / 2.5 h / 0 - 20 °C
3: 345 mg / MnO2 / CCl4 / 2 h / 20 °C
4: NaH / tetrahydrofuran / 24 h / 20 °C
5: 295 mg / tetrabutylammonium fluoride / CH2Cl2 / 1 h / 20 °C
6: 71 percent / pyridine / CH2Cl2 / 0.17 h
With
pyridine; 1H-imidazole; manganese(IV) oxide; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1021/jm0510732
- Guidance literature:
-
Multi-step reaction with 3 steps
1: NaH / tetrahydrofuran / 24 h / 20 °C
2: 295 mg / tetrabutylammonium fluoride / CH2Cl2 / 1 h / 20 °C
3: 71 percent / pyridine / CH2Cl2 / 0.17 h
With
pyridine; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0510732
![trans-6-[2-(3,4,5-trimethoxy-phenyl)-vinyl]-benzo[b]thiophen-4-ol](/Databaselist/images/loading.webp)
