2-(Triphenylstannyl)-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione

Base Information

Chemical Name:2-(Triphenylstannyl)-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione
CAS No.:83171-58-8
Molecular Formula:C₂₅H₁₉NO₃SSn
Molecular Weight:532.207
Hs Code.:
DSSTox Substance ID:DTXSID40513568

Synonyms:83171-58-8;DTXSID40513568;2-(Triphenylstannyl)-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione

Suppliers and Price of 2-(Triphenylstannyl)-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-(Triphenylstannyl)-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:533.010767
Heavy Atom Count:31
Complexity:700

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Sn](C2=CC=CC=C2)(C3=CC=CC=C3)N4C(=O)C5=CC=CC=C5S4(=O)=O

Technology Process of 2-(Triphenylstannyl)-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione

There total 1 articles about 2-(Triphenylstannyl)-1H-1lambda~6~,2-benzothiazole-1,1,3(2H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 6381-61-9
ammonium saccharin

: 639-58-7
triphenyltin chloride

: 83171-58-8
N-triphenylstannyl-4,5-benzisothiazol-3(2H)-one 1,1-dioxide

Guidance literature:: In methanol; byproducts: ammonium chloride; ammonium saccharin was added to a soln. of Ph3SnCl in anhyd. methanol, mixt. was refluxed for 1 h; filtered, filtrate evapd. in vacuo, NH4Cl was removed by washing several times with distilled water, recrystd. twice from methanol; elem. anal.;
DOI:10.1016/0022-328X(84)80135-7

Reference yield: 92.0%

: 36913-44-7
(N,N'-ethylenebis(salicylideneaminato))oxovanadium(IV)

: 83171-58-8
N-triphenylstannyl-4,5-benzisothiazol-3(2H)-one 1,1-dioxide

: VO(OC₆H₄CHNCH₂CH₂NCHC₆H₄O)Sn(C₆H₅)3(C₇H₄NO₃S)

Guidance literature:: In ethanol; N2-atmosphere; refluxing VO-complex with 1.3 equiv. of Sn-compd. for 2 h; crystn. on cooling to room temp., filtration, washing (Et2O); elem. anal.;
DOI:10.1016/S0020-1693(99)00230-3

Reference yield: 69.0%

: 29876-29-7,36537-60-7,1021603-25-7,22785-41-7
propan-1,2-diylbis(N,N'-salicylideneiminato)oxovanadium(IV)

: 83171-58-8
N-triphenylstannyl-4,5-benzisothiazol-3(2H)-one 1,1-dioxide

: VO(OC₆H₄C(CH₃)NCH(CH₃)CH₂NC(CH₃)C₆H₄O)Sn(C₆H₅)3(C₇H₄NO₃S)

Guidance literature:: In acetonitrile; N2-atmosphere; refluxing equimolar amts. for 2 h (pptn.); filtration, washing (Et2O); elem. anal.;
DOI:10.1016/S0020-1693(99)00230-3