2-Azido-4-ethenylcyclohexan-1-ol

Base Information

• Chemical Name: 2-Azido-4-ethenylcyclohexan-1-ol
• CAS No.: 83185-50-6
• Molecular Formula: C₈H₁₃N₃O
• Molecular Weight: 167.211
• DSSTox Substance ID: DTXSID30529815
• Mol file: 83185-50-6.mol

Synonyms:2-Azido-4-ethenylcyclohexan-1-ol;83185-50-6;DTXSID30529815

Chemical Property of 2-Azido-4-ethenylcyclohexan-1-ol

Chemical Property:

• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 167.105862047
• Heavy Atom Count: 12
• Complexity: 210

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CC1CCC(C(C1)N=[N+]=[N-])O

Technology Process of 2-Azido-4-ethenylcyclohexan-1-ol

There total 1 articles about 2-Azido-4-ethenylcyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

1,2-Epoxy-4-vinylcyclohexane (106-86-5) → 3,4-dihydroxy-1-vinylcyclohexane (31646-64-7) + 4-azido-3-hydroxy-1-vinylcyclohexane (83185-49-3) + 3-azido-4-hydroxy-1-vinylcyclohexane (83185-50-6)

Guidance literature:

With sodium azide; In water; at 100 ℃; for 5h;

Reference yield:

3-azido-4-hydroxy-1-vinylcyclohexane (83185-50-6) → 3-azido-4-hydroxy-1-(epoxyethyl)cyclohexane

Guidance literature:

With peracetic acid; In diethyl ether; for 336h; Ambient temperature;

Reference yield:

3-azido-4-hydroxy-1-vinylcyclohexane (83185-50-6) → 3-amino-4-hydroxy-1-vinylcyclohexane (90125-42-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 6h; Heating;

upstream raw materials:

1,2-Epoxy-4-vinylcyclohexane

Downstream raw materials:

3-amino-4-hydroxy-1-vinylcyclohexane