(6Z)-6-[(cyclohexylamino)methylidene]cyclohexa-2,4-dien-1-one - cobalt (2:1)

Base Information

Chemical Name:(6Z)-6-[(cyclohexylamino)methylidene]cyclohexa-2,4-dien-1-one - cobalt (2:1)
CAS No.:16972-55-7
Molecular Formula:C₂₆H₃₂CoN₂O₂
Molecular Weight:463.545
Hs Code.:
Mol file:16972-55-7.mol

Synonyms:Cobalt,bis[o-(N-cyclohexylformimidoyl)phenolato]- (7CI,8CI); Phenol,o-(N-cyclohexylformimidoyl)-, Co deriv. (6CI); Phenol,2-[(cyclohexylimino)methyl]-, cobalt complex;Bis(N-cyclohexylsalicylaldiminato)cobalt; NSC 151139

Suppliers and Price of (6Z)-6-[(cyclohexylamino)methylidene]cyclohexa-2,4-dien-1-one - cobalt (2:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 5 raw suppliers

Chemical Property of (6Z)-6-[(cyclohexylamino)methylidene]cyclohexa-2,4-dien-1-one - cobalt (2:1)

Chemical Property:

Vapor Pressure:4.46E-05mmHg at 25°C
Boiling Point:350.2°Cat760mmHg
Flash Point:139.5°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (6Z)-6-[(cyclohexylamino)methylidene]cyclohexa-2,4-dien-1-one - cobalt (2:1)

There total 4 articles about (6Z)-6-[(cyclohexylamino)methylidene]cyclohexa-2,4-dien-1-one - cobalt (2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19028-72-9
N-cyclohexylsalicylideneamine

: 71-48-7,917-69-1,5931-89-5,55881-15-7,68931-68-0,68931-69-1,93029-27-7
cobalt(II) acetate

: 16972-55-7
[Co(cyclohexyl-salicyl)₂]

Guidance literature:: In ethanol; water; formation out of alc. solution of salicylidene-cyclohexylamine and aq. Co-acetate-solution;;
DOI:10.1038/176832a0

Reference yield:

: {Co(C₆H₄(O)CHO)2} * dihydrate

: 108-91-8,157973-60-9
cyclohexylamine

: 16972-55-7
[Co(cyclohexyl-salicyl)₂]

Guidance literature:: In not given; formation at refluxion of a soln. of (Co(OC6H4CHO)2)*2H2O and cyclohexylamine for 1 h on a water-bath;; recrystallisation in CHCl3 and petroleum ether;;
DOI:10.1021/ja01489a014

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 90-02-8
salicylaldehyde

: 16972-55-7
[Co(cyclohexyl-salicyl)₂]

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 16 h / 20 °C / Inert atmosphere; Schlenk technique

2: methanol / Reflux; Inert atmosphere; Schlenk technique

In methanol;
DOI:10.1080/00958972.2018.1527322