5-ethoxy-6-methoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride

Base Information

Chemical Name:5-ethoxy-6-methoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride
CAS No.:63937-94-0
Molecular Formula:C₁₃H₁₉NO₂*ClH
Molecular Weight:257.76
Hs Code.:

Synonyms:Isoquinoline,5-ethoxy-1,2,3,4-tetrahydro-6-methoxy-2-methyl-, hydrochloride (9CI)

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-ethoxy-6-methoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride

Chemical Property:

Vapor Pressure:0.000254mmHg at 25°C
Boiling Point:323.9°Cat760mmHg
Flash Point:115.3°C
Density:g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-ethoxy-6-methoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride

There total 4 articles about 5-ethoxy-6-methoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87790-87-2
1-Amino-2-(2-ethoxy-3-methoxyphenyl)-ethan

: 63937-94-0
5-ethoxy-6-methoxy-2-methyl-1,2,3,4-tetrahydro-isoquinoline; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: benzaldehyde / Beim Erwaermen des Kondensationsprodukts mit Methyljodid und Erwaermen des Reaktionsprodukts mit wasserhaltigem Aethanol

2: water / und Erwaermen des Reaktionsprodukts mit konz. Salzsaeure

With water; benzaldehyde;
DOI:10.1021/ja01283a038

Reference yield:

: 858783-48-9
3-(2-ethoxy-3-methoxy-phenyl)-propionic acid amide

: 63937-94-0
5-ethoxy-6-methoxy-2-methyl-1,2,3,4-tetrahydro-isoquinoline; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hypochlorite

2: benzaldehyde / Beim Erwaermen des Kondensationsprodukts mit Methyljodid und Erwaermen des Reaktionsprodukts mit wasserhaltigem Aethanol

3: water / und Erwaermen des Reaktionsprodukts mit konz. Salzsaeure

With sodium hypochlorite; water; benzaldehyde;
DOI:10.1021/ja01283a038

Reference yield:

: 873422-29-8
3-(2-ethoxy-3-methoxy-phenyl)-propionic acid

: 63937-94-0
5-ethoxy-6-methoxy-2-methyl-1,2,3,4-tetrahydro-isoquinoline; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: ammonia / 220 - 230 °C

2: sodium hypochlorite

3: benzaldehyde / Beim Erwaermen des Kondensationsprodukts mit Methyljodid und Erwaermen des Reaktionsprodukts mit wasserhaltigem Aethanol

4: water / und Erwaermen des Reaktionsprodukts mit konz. Salzsaeure

With sodium hypochlorite; ammonia; water; benzaldehyde;
DOI:10.1021/ja01283a038