5H-Benzo[f]pyrano[2,3-h]quinoxaline, 6,7-dihydro-7,7-dimethyl-

Base Information

• Chemical Name: 5H-Benzo[f]pyrano[2,3-h]quinoxaline, 6,7-dihydro-7,7-dimethyl-
• CAS No.: 833122-18-2
• Molecular Formula: C17H16N2O
• Molecular Weight: 264.327
• ChEMBL ID: CHEMBL448792
• DSSTox Substance ID: DTXSID30479508
• Nikkaji Number: J2.132.826J
• Wikidata: Q82313588
• Mol file: 833122-18-2.mol

Synonyms:833122-18-2;5H-Benzo[f]pyrano[2,3-h]quinoxaline, 6,7-dihydro-7,7-dimethyl-;CHEMBL448792;MTTCJOLBNDKEAW-UHFFFAOYSA-;DTXSID30479508;7,7-dimethyl-6,7-dihydro-5h-benzo[f]pyrano[2,3-h]quinoxaline;InChI=1/C17H16N2O/c1-17(2)8-7-13-15-14(18-9-10-19-15)11-5-3-4-6-12(11)16(13)20-17/h3-6,9-10H,7-8H2,1-2H3

Chemical Property of 5H-Benzo[f]pyrano[2,3-h]quinoxaline, 6,7-dihydro-7,7-dimethyl-

Chemical Property:

• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 264.126263138
• Heavy Atom Count: 20
• Complexity: 370

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CCC2=C(O1)C3=CC=CC=C3C4=NC=CN=C24)C

Technology Process of 5H-Benzo[f]pyrano[2,3-h]quinoxaline, 6,7-dihydro-7,7-dimethyl-

There total 1 articles about 5H-Benzo[f]pyrano[2,3-h]quinoxaline, 6,7-dihydro-7,7-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,2-dimethyl-3,4-dihydro-2H-benzo[h]chromene-5,6-dione (4707-32-8) + ethylenediamine (107-15-3,85404-18-8) → 5,6-dihydro-7,7-dimethyl-7H-pyrano[3',2':4]naphtha[1,2-b]pyrazine (833122-18-2)

Guidance literature:

at 20 ℃; for 24h;

DOI:10.1080/00397910600978507

Reference yield: 68.0%

5,6-dihydro-7,7-dimethyl-7H-pyrano[3',2':4]naphtha[1,2-b]pyrazine (833122-18-2) → 8,8-dimethyl-7,8-dihydro-6H-[2]benzoxecino[7,8-b]pyrazine-5,10-dione

Guidance literature:

With dihydrogen peroxide; acetic anhydride; In chloroform; water; at 20 ℃; for 24h;

DOI:10.1016/j.ejmech.2008.06.014

Reference yield: 20.5%

5,6-dihydro-7,7-dimethyl-7H-pyrano[3',2':4]naphtha[1,2-b]pyrazine (833122-18-2) → 8,8-dimethyl-7,8-dihydro-6H-[2]benzoxecino[7,8-b]pyrazine-5,10-dione + 5-(3-hydroxy-3-methylbutyl)-5-hydroxybenzo[f]quinoxalin-6(5H)-one-4-N-oxide

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 72h;

DOI:10.1007/s10870-006-9097-1

upstream raw materials:

2,2-dimethyl-3,4-dihydro-2H-benzo[h]chromene-5,6-dione

ethylenediamine