2,7,8-Trimethyl-1-phenyl-1H-purin-6(7H)-one

Base Information

Chemical Name:2,7,8-Trimethyl-1-phenyl-1H-purin-6(7H)-one
CAS No.:83325-09-1
Molecular Formula:C₁₄H₁₄N₄O
Molecular Weight:254.291
Hs Code.:
DSSTox Substance ID:DTXSID40513861
Wikidata:Q82373868

Synonyms:83325-09-1;2,7,8-Trimethyl-1-phenyl-1H-purin-6(7H)-one;2,7,8-trimethyl-1-phenyl-6,7-dihydro-1H-purin-6-one;DTXSID40513861;2,7,8-Trimethyl-1-phenyl-1,7-dihydro-6H-purin-6-one

Suppliers and Price of 2,7,8-Trimethyl-1-phenyl-1H-purin-6(7H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,7,8-Trimethyl-1-phenyl-1H-purin-6(7H)-one

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:254.11676108
Heavy Atom Count:19
Complexity:402

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC2=C(N1C)C(=O)N(C(=N2)C)C3=CC=CC=C3

Technology Process of 2,7,8-Trimethyl-1-phenyl-1H-purin-6(7H)-one

There total 2 articles about 2,7,8-Trimethyl-1-phenyl-1H-purin-6(7H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 142-04-1,36663-09-9
aniline hydrochloride

: 83325-23-9
5-Acetylamino-2,3-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester

: 83325-09-1
1,7-dihydro-1-phenyl-2,7,8-trimethyl-6H-purin-6-one

Guidance literature:: With N,N-dimethyl-cyclohexanamine; phosphorus pentoxide; at 150 ℃; for 2h;
DOI:10.1016/0040-4020(82)80226-3

Reference yield:

: 55747-02-9
4-amino-1,2-dimethyl-1H-imidazole-5-carboxylic acid ethyl ester

: 83325-09-1
1,7-dihydro-1-phenyl-2,7,8-trimethyl-6H-purin-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / acetic acid / 2 h / Heating

2: 46 percent / N,N-dimethylcyclohexylamine, P₂O₅ / 2 h / 150 °C

With N,N-dimethyl-cyclohexanamine; phosphorus pentoxide; In acetic acid;
DOI:10.1016/0040-4020(82)80226-3