benzyl 4-mercaptopiperidine-1-carboxylate

Base Information

Chemical Name:benzyl 4-mercaptopiperidine-1-carboxylate
CAS No.:833491-24-0
Molecular Formula:C13H17NO2S
Molecular Weight:251.349
Hs Code.:
Mol file:833491-24-0.mol

Synonyms:benzyl 4-mercaptopiperidine-1-carboxylate;1-Piperidinecarboxylic acid,4-mercapto-,phenylmethyl ester;4-Mercapto-piperidine-1-carboxylic acid benzyl ester;

Suppliers and Price of benzyl 4-mercaptopiperidine-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-Mercapto-piperidine-1-carboxylicacidbenzylester 95+%
1g
$ 1113.00

Chemenu
benzyl4-mercaptopiperidine-1-carboxylate 95%
1g
$ 930.00

Alichem
4-Mercapto-piperidine-1-carboxylicacidbenzylester
1g
$ 1090.74

Total 9 raw suppliers

Chemical Property of benzyl 4-mercaptopiperidine-1-carboxylate

Chemical Property:

PSA：68.34000
LogP:2.65530

Purity/Quality:

97% ^*data from raw suppliers

4-Mercapto-piperidine-1-carboxylicacidbenzylester 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 4-mercaptopiperidine-1-carboxylate

There total 2 articles about benzyl 4-mercaptopiperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 146827-60-3
4-(acetylthio)-1-(benzyloxycarbonyl)piperidine

: 833491-24-0
benzyl 4-mercaptopiperidine-1-carboxylate

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 1.5h;

Reference yield:

: 95798-23-5
1-(benzyloxycarbonyl)-4-hydroxypiperidine

: 833491-24-0
benzyl 4-mercaptopiperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanesulfonyl chloride; triethylamine / dichloromethane / 48 h / 0 - 20 °C

1.2: 3 h / 90 °C

2.1: sodium tetrahydroborate / methanol / 1.5 h / 0 - 20 °C

With sodium tetrahydroborate; methanesulfonyl chloride; triethylamine; In methanol; dichloromethane;

Reference yield:

: 833491-24-0
benzyl 4-mercaptopiperidine-1-carboxylate

: 89151-45-1
tert-butyl-4-(2-(tosyloxy)ethyl)piperidine-1-carboxylate

: 833491-25-1
tert-butyl 4-[2-({1-[(benzyloxy)carbonyl]piperidin-4-yl}sulfonyl)ethyl]piperidine-1-carboxylate

Guidance literature:: benzyl 4-mercaptopiperidine-1-carboxylate; With sodium hydride; at 0 - 20 ℃; for 0.5h;

tert-butyl-4-(2-(tosyloxy)ethyl)piperidine-1-carboxylate; In DMF (N,N-dimethyl-formamide); for 16h;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 48h;