Cyclo(D-alanyl-L-alanyl-N-methyl-L-tyrosyl-L-alanyl-N-methyl-L-tyrosyl-3-hydroxy-N,O-dimethyl-L-tyrosyl),cyclic (5®6)-ether

Base Information

Chemical Name:Cyclo(D-alanyl-L-alanyl-N-methyl-L-tyrosyl-L-alanyl-N-methyl-L-tyrosyl-3-hydroxy-N,O-dimethyl-L-tyrosyl),cyclic (5®6)-ether
CAS No.:106235-26-1
Molecular Formula:C40H48 N6 O9
Molecular Weight:756.856
Hs Code.:

Synonyms:Bouvardin,3-(N-methyl-L-tyrosine)-5-(N-methyl-L-tyrosine)-6-(3-hydroxy-N,O-dimethyl-L-tyrosine)-(9CI);22-Oxa-3,6,9,12,15,29-hexaazatetracyclo[14.12.2.218,21.123,27]tritriacontane,cyclic peptide deriv.; RA II

Suppliers and Price of Cyclo(D-alanyl-L-alanyl-N-methyl-L-tyrosyl-L-alanyl-N-methyl-L-tyrosyl-3-hydroxy-N,O-dimethyl-L-tyrosyl),cyclic (5®6)-ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cyclo(D-alanyl-L-alanyl-N-methyl-L-tyrosyl-L-alanyl-N-methyl-L-tyrosyl-3-hydroxy-N,O-dimethyl-L-tyrosyl),cyclic (5®6)-ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclo(D-alanyl-L-alanyl-N-methyl-L-tyrosyl-L-alanyl-N-methyl-L-tyrosyl-3-hydroxy-N,O-dimethyl-L-tyrosyl),cyclic (5®6)-ether

There total 1 articles about Cyclo(D-alanyl-L-alanyl-N-methyl-L-tyrosyl-L-alanyl-N-methyl-L-tyrosyl-3-hydroxy-N,O-dimethyl-L-tyrosyl),cyclic (5®6)-ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: RA-V

: 18107-18-1
diazomethyl-trimethyl-silane

: 64725-24-2
deoxybouvadin

: 122621-60-7,144993-87-3,144993-88-4,86229-97-2
RA-VII

: 106235-26-1
RA-II

Guidance literature:: With dmap; In methanol; hexane; acetonitrile; for 21h; Ambient temperature;
DOI:10.1039/p19960000213

Reference yield: 99.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 106235-26-1
RA-II

: 174580-19-9
RA-II O-triflate

Guidance literature:: With triethylamine; In dichloromethane; for 26h; Ambient temperature;
DOI:10.1039/p19960000213

Reference yield:

: 106235-26-1
RA-II

: (ζ-Ethyl-N-methylphenylalanine-3)RA-VII

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 26 h / Ambient temperature

2: 87 percent / LiCl, dichlorobis(triphenylphosphine)palladium(II) / dimethylformamide / 49 h / 80 °C

3: 92 percent / H₂ / 10percent Pd/C / ethanol / 1 h / Ambient temperature

With bis-triphenylphosphine-palladium(II) chloride; hydrogen; triethylamine; lithium chloride; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/p19960000213