octahydro-1H-pyrrolo[1,2-a]azepine

Base Information

• Chemical Name: octahydro-1H-pyrrolo[1,2-a]azepine
• CAS No.: 5715-05-9
• Molecular Formula: C9H17N
• Molecular Weight: 139.238

Synonyms:

Chemical Property of octahydro-1H-pyrrolo[1,2-a]azepine

Chemical Property:

• Vapor Pressure: 0.471mmHg at 25°C
• Boiling Point: 193.2°Cat760mmHg
• Flash Point: 63.1°C
• Density: 0.94g/cm³

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of octahydro-1H-pyrrolo[1,2-a]azepine

There total 24 articles about octahydro-1H-pyrrolo[1,2-a]azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1,2,3,5,6,7,8,9-octahydro-1H-pyrrolo[1,2-a]azepinylium chloride → 1-azabicyclo[5.3.0]decane (5715-05-9,378248-39-6)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 0.75h;

DOI:10.1016/S0040-4020(03)00375-2

Reference yield: 10.0%

nonamethyleneimine (4396-27-4) → quinolizidine (493-10-7) + 1-azabicyclo[5.3.0]decane (5715-05-9,378248-39-6)

Guidance literature:

With lithium bromide; In water; acetonitrile; for 3h; electrochemical oxidation, C anode, 100 mA;

Reference yield:

→ 1-azabicyclo[5.3.0]decane (5715-05-9,378248-39-6)

Guidance literature:

With 1,4-dioxane; copper oxide-chromium oxide; at 265 ℃; under 257428 Torr; Hydrogenation;

DOI:10.1021/ja01168a010

upstream raw materials:

nonamethyleneimine

hydrogenchloride

hexahydro-quinolizin-1-one

water

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