1,2-Cyclohexanediamine, N-methyl-N-(phenylmethyl)-, (1R,2R)-

Base Information

Chemical Name:1,2-Cyclohexanediamine, N-methyl-N-(phenylmethyl)-, (1R,2R)-
CAS No.:834917-67-8
Molecular Formula:C14H22N2
Molecular Weight:218.342
Hs Code.:
DSSTox Substance ID:DTXSID20478747
Nikkaji Number:J2.617.034F
Wikidata:Q82312319

Synonyms:834917-67-8;1,2-Cyclohexanediamine, N-methyl-N-(phenylmethyl)-, (1R,2R)-;DTXSID20478747;AKOS005264488;(1R,2R)-1-N-benzyl-1-N-methylcyclohexane-1,2-diamine

Suppliers and Price of 1,2-Cyclohexanediamine, N-methyl-N-(phenylmethyl)-, (1R,2R)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Cyclohexanediamine, N-methyl-N-(phenylmethyl)-, (1R,2R)-

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:218.178298710
Heavy Atom Count:16
Complexity:199

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(CC1=CC=CC=C1)C2CCCCC2N
Isomeric SMILES:CN(CC1=CC=CC=C1)[C@@H]2CCCC[C@H]2N

Technology Process of 1,2-Cyclohexanediamine, N-methyl-N-(phenylmethyl)-, (1R,2R)-

There total 6 articles about 1,2-Cyclohexanediamine, N-methyl-N-(phenylmethyl)-, (1R,2R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2-{(1R,2R)-2-(N-benzyl-N-methylamino)cyclohexyl}isoindoline-1,3-dione

: 834917-67-8
(1R,2R)-N¹-benzyl-N¹-methylcyclohexane-1,2-diamine

Guidance literature:: With hydrazine hydrate; In ethanol; for 0.75h; Heating;
DOI:10.1039/b607574f

Reference yield:

: 1523095-43-3
C₁₉H₃₀N₂O₂

: 834917-67-8
(1R,2R)-N¹-benzyl-N¹-methylcyclohexane-1,2-diamine

Guidance literature:: C₁₉H₃₀N₂O₂; With hydrogenchloride; In water; at 20 ℃; for 12h;

With sodium hydroxide; In dichloromethane; water; pH=13;
DOI:10.1016/j.tetasy.2013.09.026

Reference yield:

: 146504-07-6
tert-butyl ((1R,2R)-2-aminocyclohexyl)carbamate

: 834917-67-8
(1R,2R)-N¹-benzyl-N¹-methylcyclohexane-1,2-diamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol / 0.5 h / 20 °C

2.1: sodium tetrahydroborate / methanol / 2.5 h / 0 °C

3.1: sodium cyanoborohydride / methanol / 5 h / 20 °C

4.1: hydrogenchloride / water / 12 h / 20 °C

4.2: pH 13

With hydrogenchloride; sodium tetrahydroborate; sodium cyanoborohydride; In methanol; water;
DOI:10.1016/j.tetasy.2013.09.026