Benzeneacetaldehyde, 3,4-dimethoxy-a-(2-oxopropyl)-

Base Information

Chemical Name:Benzeneacetaldehyde, 3,4-dimethoxy-a-(2-oxopropyl)-
CAS No.:838846-30-3
Molecular Formula:C13H16O4
Molecular Weight:236.268
Hs Code.:

Synonyms:

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Chemical Property of Benzeneacetaldehyde, 3,4-dimethoxy-a-(2-oxopropyl)-

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Technology Process of Benzeneacetaldehyde, 3,4-dimethoxy-a-(2-oxopropyl)-

There total 3 articles about Benzeneacetaldehyde, 3,4-dimethoxy-a-(2-oxopropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 77783-92-7
(+/-)-2-(3,4-dimethoxyphenyl)penten-4-al

: 838846-30-3
2-(3,4-dimethoxy-phenyl)-4-oxo-pentanal

Guidance literature:: With potassium bromate; palladium 10% on activated carbon; In tetrahydrofuran; water; at 65 ℃;
DOI:10.1016/j.tetlet.2013.01.082

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 838846-30-3
2-(3,4-dimethoxy-phenyl)-4-oxo-pentanal

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 1 h / 0 °C

2: 95 percent / xylene / Heating

3: aq. CuCl₂; O₂ / PdCl₂ / 1,2-dimethoxy-ethane / 20 °C

With potassium tert-butylate; oxygen; copper dichloride; palladium dichloride; In tetrahydrofuran; 1,2-dimethoxyethane; xylene; tert-butyl alcohol; 1: Wittig olefination / 2: Claisen rearrangement / 3: Wacker oxidation;
DOI:10.1055/s-2004-831208

Reference yield:

: 188476-12-2
4-((E)-2-Allyloxy-vinyl)-1,2-dimethoxy-benzene

: 838846-30-3
2-(3,4-dimethoxy-phenyl)-4-oxo-pentanal

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / xylene / Heating

2: aq. CuCl₂; O₂ / PdCl₂ / 1,2-dimethoxy-ethane / 20 °C

With oxygen; copper dichloride; palladium dichloride; In 1,2-dimethoxyethane; xylene; 1: Claisen rearrangement / 2: Wacker oxidation;
DOI:10.1055/s-2004-831208