3-(2-Iodoethyl)-3-methyloxetane

Base Information

Chemical Name:3-(2-Iodoethyl)-3-methyloxetane
CAS No.:84078-62-6
Molecular Formula:C6H11IO
Molecular Weight:226.05500
Hs Code.:2932990090
DSSTox Substance ID:DTXSID50693527
Wikidata:Q82622579
Mol file:84078-62-6.mol

Synonyms:3-(2-iodoethyl)-3-methyloxetane;84078-62-6;Oxetane, 3-(2-iodoethyl)-3-methyl-;DTXSID50693527;AKOS015907076;FT-0739535

Suppliers and Price of 3-(2-Iodoethyl)-3-methyloxetane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-(2-Iodoethyl)-3-methyloxetane

Chemical Property:

Boiling Point:207.6±13.0 °C(Predicted)
PSA：9.23000
Density:1.651±0.06 g/cm3(Predicted)
LogP:1.84800
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:225.98546
Heavy Atom Count:8
Complexity:78.6

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(COC1)CCI

Technology Process of 3-(2-Iodoethyl)-3-methyloxetane

There total 1 articles about 3-(2-Iodoethyl)-3-methyloxetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: Toluene-4-sulfonic acid 2-(3-methyl-oxetan-3-yl)-ethyl ester

: 84078-62-6
3-(2-iodoethyl)-3-methyloxetane

Guidance literature:: With sodium iodide; In acetone; Heating;
DOI:10.1039/P19830001783

Reference yield: 78.0%

: 84078-62-6
3-(2-iodoethyl)-3-methyloxetane

: 84078-61-5
1-(2-phenylsulphonylethyl)-2-methylene-6,6-dimethylcyclohexane

: 84078-63-7
3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 2.) 20 deg C, 2 h;
DOI:10.1039/P19830001783

Reference yield:

: 84078-62-6
3-(2-iodoethyl)-3-methyloxetane

: 84078-65-9
6-(2-methylene-6,6-dimethylcyclohexyl)-5-methylene-2,2-dimethylhexan-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / 1.3M-n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 2.) 20 deg C, 2 h

2: 65 percent / lithium di-isopropylamide / tetrahydrofuran; hexane / -78 deg C -> -10 deg C

3: 1.11 g / Et₃N / CH₂Cl₂

4: 0.43 g / 5.65percent Na(Hg) / tetrahydrofuran; methanol / 4 h / -10 °C

5: 95 percent / ethylenediamine, Li / diethyl ether / 0.5 h

With n-butyllithium; sodium amalgam; lithium; ethylenediamine; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane;
DOI:10.1039/P19830001783