(1,1-Dichloro-3-methylbut-2-ene-1-sulfonyl)benzene

Base Information

Chemical Name:(1,1-Dichloro-3-methylbut-2-ene-1-sulfonyl)benzene
CAS No.:84602-94-8
Molecular Formula:C11H12Cl2O2S
Molecular Weight:279.187
Hs Code.:
DSSTox Substance ID:DTXSID80517464

Synonyms:84602-94-8;(1,1-Dichloro-3-methylbut-2-ene-1-sulfonyl)benzene;DTXSID80517464

Suppliers and Price of (1,1-Dichloro-3-methylbut-2-ene-1-sulfonyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1,1-Dichloro-3-methylbut-2-ene-1-sulfonyl)benzene

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:277.9935062
Heavy Atom Count:16
Complexity:356

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC(S(=O)(=O)C1=CC=CC=C1)(Cl)Cl)C

Technology Process of (1,1-Dichloro-3-methylbut-2-ene-1-sulfonyl)benzene

There total 3 articles about (1,1-Dichloro-3-methylbut-2-ene-1-sulfonyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 15874-80-3
3-methyl-1-(phenylsulfonyl)but-2-ene

: 84602-94-8
1,1-dichloro-3-methyl-2-butenyl phenyl sulfone

Guidance literature:: With sodium hydroxide; hexachloroethane; tetrabutylammomium bromide; In dichloromethane; at 20 - 45 ℃; for 1h;

Reference yield: 60.0%

: 56-23-5
tetrachloromethane

: 15874-80-3
3-methyl-1-(phenylsulfonyl)but-2-ene

: 84602-94-8
1,1-dichloro-3-methyl-2-butenyl phenyl sulfone

: 84602-96-0
[Dichloro-(2-chloro-3,3-dimethyl-cycloprop-1-enyl)-methanesulfonyl]-benzene

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide;
DOI:10.1021/jo00154a042

Reference yield:

: 873-55-2
sodium benzenesulfonate

: 84602-94-8
1,1-dichloro-3-methyl-2-butenyl phenyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / dimethylsulfoxide / 5 h / 65 - 70 °C

2: 96 percent / hexachloroethane, 50percent aq. NaOH, tetrabutylammonium bromide / CH₂Cl₂ / 1 h / 20 - 45 °C

With sodium hydroxide; hexachloroethane; tetrabutylammomium bromide; In dichloromethane; dimethyl sulfoxide;