9-(4-Methoxyphenyl)-9H-carbazole-3-carbaldehyde

Base Information

Chemical Name:9-(4-Methoxyphenyl)-9H-carbazole-3-carbaldehyde
CAS No.:84746-66-7
Molecular Formula:C20H15NO2
Molecular Weight:301.345
Hs Code.:2933990090
DSSTox Substance ID:DTXSID40465573
Nikkaji Number:J211.578F
Wikidata:Q82291622
Mol file:84746-66-7.mol

Synonyms:9-(4-Methoxyphenyl)-9H-carbazole-3-carbaldehyde;84746-66-7;9-(4-methoxyphenyl)carbazole-3-carbaldehyde;SCHEMBL7145772;DTXSID40465573

Suppliers and Price of 9-(4-Methoxyphenyl)-9H-carbazole-3-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 9-(4-Methoxyphenyl)-9H-carbazole-3-carbaldehyde

Chemical Property:

PSA：31.23000
LogP:4.60480
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:301.110278721
Heavy Atom Count:23
Complexity:418

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N2C3=C(C=C(C=C3)C=O)C4=CC=CC=C42

Technology Process of 9-(4-Methoxyphenyl)-9H-carbazole-3-carbaldehyde

There total 4 articles about 9-(4-Methoxyphenyl)-9H-carbazole-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 19264-74-5
9-(4-methoxyphenyl)-9H-carbazole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 84746-66-7
9-(4-methoxyphenyl)-9H-carbazole-3-carbaldehyde

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; at 20 ℃; for 1h; Inert atmosphere;

9-(4-methoxyphenyl)-9H-carbazole; at 90 ℃; for 120h; Inert atmosphere;
DOI:10.1039/c5ta04991a

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 84746-66-7
9-(4-methoxyphenyl)-9H-carbazole-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide; L-proline / dimethyl sulfoxide / 48 h / 120 °C / Inert atmosphere

2.1: trichlorophosphate / 1 h / 20 °C / Inert atmosphere

2.2: 120 h / 90 °C / Inert atmosphere

With copper(l) iodide; L-proline; trichlorophosphate; In dimethyl sulfoxide; 2.1: |Vilsmeier-Haack Formylation / 2.2: |Vilsmeier-Haack Formylation;
DOI:10.1039/c5ta04991a

Reference yield:

: 696-62-8
para-iodoanisole

: 84746-66-7
9-(4-methoxyphenyl)-9H-carbazole-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; copper(I) oxide / N,N-dimethyl acetamide

2: trichlorophosphate / dichloromethane

With copper(I) oxide; potassium carbonate; trichlorophosphate; In dichloromethane; N,N-dimethyl acetamide;
DOI:10.1016/j.molliq.2018.11.164