6,7-Dimethoxy-2-methylisoquinolin-2-ium iodide

Base Information

Chemical Name:6,7-Dimethoxy-2-methylisoquinolin-2-ium iodide
CAS No.:3428-75-9
Molecular Formula:C12H14NO2+
Molecular Weight:204.2445
Hs Code.:
NSC Number:166737
DSSTox Substance ID:DTXSID90372884

Synonyms:3428-75-9;6,7-dimethoxy-2-methylisoquinolin-2-ium iodide;DTXSID90372884;NSC166737;AKOS004901637;NSC-166737;2-methyl-6,7-dimethoxyisoquinolinium iodide

Suppliers and Price of 6,7-Dimethoxy-2-methylisoquinolin-2-ium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 6,7-Dimethoxy-2-methylisoquinolin-2-ium iodide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:331.00693
Heavy Atom Count:16
Complexity:210

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[N+]1=CC2=CC(=C(C=C2C=C1)OC)OC.[I-]

Technology Process of 6,7-Dimethoxy-2-methylisoquinolin-2-ium iodide

There total 5 articles about 6,7-Dimethoxy-2-methylisoquinolin-2-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 15248-39-2
6,7-dimethoxyisoquinoline

: 74-88-4
methyl iodide

: 3428-75-9
N-methyl-6,7-dimethoxyisoquinolinium iodide

Guidance literature:: for 1h; Heating;

Reference yield:

: 3382-18-1
6,7-dimethoxy-3,4-dihydro-isoquinoline

: 3428-75-9
N-methyl-6,7-dimethoxyisoquinolinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / 10 percent Pd/C / decahydronaphthalene / 1.5 h / 190 °C

2: 93 percent / 1 h / Heating

With palladium on activated charcoal; In decalin;

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 3428-75-9
N-methyl-6,7-dimethoxyisoquinolinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃ / 2.5 h / 190 - 200 °C

2: 30 percent / 10 percent Pd/C / decahydronaphthalene / 1.5 h / 190 °C

3: 93 percent / 1 h / Heating

With palladium on activated charcoal; trichlorophosphate; In decalin;