Benzoyl chloride, 3,5-bis(chlorosulfonyl)-

Base Information

• Chemical Name: Benzoyl chloride, 3,5-bis(chlorosulfonyl)-
• CAS No.: 37828-01-6
• Molecular Formula: C7H3 Cl3 O5 S2
• Molecular Weight: 337.589
• Hs Code.: 2916399090
• European Community (EC) Number: 253-678-7
• UNII: W8DZ2VY53J
• DSSTox Substance ID: DTXSID2068052
• Nikkaji Number: J261.252F
• Wikidata: Q81994754
• Mol file: 37828-01-6.mol

Synonyms:3,5-bis(chlorosulfonyl)benzoyl chloride;37828-01-6;Benzoyl chloride, 3,5-bis(chlorosulfonyl)-;3,5-Bis(chlorosulphonyl)benzoyl chloride;EINECS 253-678-7;W8DZ2VY53J;UNII-W8DZ2VY53J;C7H3Cl3O5S2;SCHEMBL4598484;DTXSID2068052;C7-H3-Cl3-O5-S2;3,5-bis(chloranylsulfonyl)benzoyl chloride;3,5-DI(CHLOROSULFONYL)BENZOYL CHLORIDE;A826654;A937205

Chemical Property of Benzoyl chloride, 3,5-bis(chlorosulfonyl)-

Chemical Property:

• Vapor Pressure: 1.31E-09mmHg at 25°C
• Boiling Point: 486.3°Cat760mmHg
• Flash Point: 247.9°C
• PSA: 102.11000
• Density: 1.784g/cm³
• LogP: 4.08220
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 335.848749
• Heavy Atom Count: 17
• Complexity: 461

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=C(C=C(C=C1S(=O)(=O)Cl)S(=O)(=O)Cl)C(=O)Cl
• Uses: 3,5-Bis(chlorosulfonyl)benzoyl Chloride is used in preparation of of 3,5-Dichlorobenzoyl Chloride.

Technology Process of Benzoyl chloride, 3,5-bis(chlorosulfonyl)-

There total 4 articles about Benzoyl chloride, 3,5-bis(chlorosulfonyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-disulfonylbenzoyl chloride → 3,5-dichlorosulfonylbenzoyl chloride (37828-01-6)

Guidance literature:

With thionyl chloride; benzamide; at 65 ℃; for 2h;

Reference yield:

→ 3,5-dichlorosulfonylbenzoyl chloride (37828-01-6)

Guidance literature:

With phosphorus trichloride; at 130 ℃;

Reference yield:

benzoyl chloride (98-88-4) → 3,5-dichlorosulfonylbenzoyl chloride (37828-01-6)

Guidance literature:

Multi-step reaction with 2 steps

1: chlorosulfonic acid / 5.5 h / 80 °C

2: thionyl chloride; benzamide / 2 h / 65 °C

With chlorosulfonic acid; thionyl chloride; benzamide;

upstream raw materials:

benzoyl chloride

Downstream raw materials:

3,5-bis-chlorosulfonyl-benzoic acid

3,5-dichlorobenzoyl chloride

Methyl 3,5-bis(chlorosulfonyl)benzoate

5-(2-hydroxy-4-methyl-phenylcarbamoyl)-benzene-1,3-disulfonic acid

Refernces

• 1、 Gal-Or,Mellema,Moudrianakis,Beer. "Electron microscopic study of base sequence in nucleic acids. VII. Cytosine-specific addition of acyl hydrazides.". . p. 1909 - 1915. Retrieved 2007/10/04.