Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[[(4-nitrophenyl)amino]carbonyl]oxy]methyl]phenyl ester

Base Information

Chemical Name:Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[[(4-nitrophenyl)amino]carbonyl]oxy]methyl]phenyl ester
CAS No.:848826-73-3
Molecular Formula:C40H42N8O16
Molecular Weight:890.817
Hs Code.:

Carbamic acid,
[2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-,
2,4,6-tris[[[[(4-nitrophenyl)amino]carbonyl]oxy]methyl]phenyl ester

Synonyms:

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Chemical Property of Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[[(4-nitrophenyl)amino]carbonyl]oxy]methyl]phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[[(4-nitrophenyl)amino]carbonyl]oxy]methyl]phenyl ester

There total 9 articles about Carbamic acid, [2-[[(1,1-dimethylethoxy)carbonyl]methylamino]ethyl]methyl-, 2,4,6-tris[[[[(4-nitrophenyl)amino]carbonyl]oxy]methyl]phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 848826-54-0
methyl-{2-[methyl-(2,4,6-tris-hydroxymethyl-phenoxycarbonyl)-amino]-ethyl}-carbamic acid tert-butyl ester

: 51028-38-7
(4-nitro-phenyl)-carbamoyl chloride

: 848826-73-3
methyl-(2-{methyl-[2,4,6-tris-(4-nitro-phenylcarbamoyloxymethyl)-phenoxycarbonyl]-amino}-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: With dmap; In ethyl acetate; at 20 ℃;

Reference yield:

: 848826-46-0
2,6-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-hydroxymethyl-phenol

: 848826-73-3
methyl-(2-{methyl-[2,4,6-tris-(4-nitro-phenylcarbamoyloxymethyl)-phenoxycarbonyl]-amino}-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 79 percent / dimethylformamide / 0.5 h / 20 °C

2: 94 percent / 4-(dimethylamino)pyridine; triethylamine / ethyl acetate / 1 h / 20 °C

3: 88 percent / dimethylformamide / 0.67 h / 20 °C

4: 90 percent / Amberlyst 15 / methanol / 2 h / 20 °C

5: 810 mg / 4-(dimethylamino)pyridine / ethyl acetate / 20 °C

With dmap; Amberlyst 15; triethylamine; In methanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 848826-44-8
3,5-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-hydroxy-benzoic acid ethyl ester

: 848826-73-3
methyl-(2-{methyl-[2,4,6-tris-(4-nitro-phenylcarbamoyloxymethyl)-phenoxycarbonyl]-amino}-ethyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / diisobutylaluminium hydride / dimethylformamide / 2 h / -78 °C

2: 79 percent / dimethylformamide / 0.5 h / 20 °C

3: 94 percent / 4-(dimethylamino)pyridine; triethylamine / ethyl acetate / 1 h / 20 °C

4: 88 percent / dimethylformamide / 0.67 h / 20 °C

5: 90 percent / Amberlyst 15 / methanol / 2 h / 20 °C

6: 810 mg / 4-(dimethylamino)pyridine / ethyl acetate / 20 °C

With dmap; Amberlyst 15; diisobutylaluminium hydride; triethylamine; In methanol; ethyl acetate; N,N-dimethyl-formamide;