4-Prenyldihydropinosylvin

Base Information

Chemical Name:4-Prenyldihydropinosylvin
CAS No.:70610-11-6
Molecular Formula:C19H22O2
Molecular Weight:282.3768
Hs Code.:
DSSTox Substance ID:DTXSID60331923
Nikkaji Number:J357.710D
Wikidata:Q27105528
Metabolomics Workbench ID:27982

Synonyms:4-Prenyldihydropinosylvin;70610-11-6;2-(3-methylbut-2-enyl)-5-(2-phenylethyl)benzene-1,3-diol;CHEBI:1926;SCHEMBL4742069;DTXSID60331923;LMPK13090041;3,5-dihydroxy-4-(3-methyl-2-butenyl)bibenzyl;Q27105528

Suppliers and Price of 4-Prenyldihydropinosylvin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-Prenyldihydropinosylvin

Chemical Property:

Vapor Pressure:2.95E-08mmHg at 25°C
Boiling Point:437.3°Cat760mmHg
Flash Point:200.5°C
Density:1.104g/cm³
XLogP3:5.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:282.161979940
Heavy Atom Count:21
Complexity:315

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCC1=C(C=C(C=C1O)CCC2=CC=CC=C2)O)C

Technology Process of 4-Prenyldihydropinosylvin

There total 7 articles about 4-Prenyldihydropinosylvin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 133156-37-3
1,3-Bis(methoxymethoxy)-2-(3-methyl-2-butenyl)-5-phenethylbenzol

: 70610-11-6
3,5-dihydroxy-4-(3-methyl-2-butenyl)-bibenzyl

Guidance literature:: With hydrogenchloride; In ethanol; at 20 ℃; for 12h;
DOI:10.1055/s-1991-26390

Reference yield:

: 24131-31-5
3,5-dibenzyloxybenzyl alcohol

: 70610-11-6
3,5-dihydroxy-4-(3-methyl-2-butenyl)-bibenzyl

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / SOCl₂, pyridine / toluene / 1) 15 min, -15 deg C 2) 30 min, reflux

2: 200 °C

3: NaOMe / dimethylformamide / 0.5 h / 80 °C

4: 98 percent / H₂ / 5percent Pd/C / ethyl acetate / 3 h / 20 °C / 3750.3 Torr

5: 1) NaH / 1) DMF, 20 deg C 2) 20 deg C, 1 h

6: 1) BuLi / 1) THF, hexane, 3 h, reflux 2) 12 h, reflux

7: 90 percent / 3percent HCl / ethanol / 12 h / 20 °C

With pyridine; hydrogenchloride; n-butyllithium; thionyl chloride; hydrogen; sodium methylate; sodium hydride; palladium on activated charcoal; In ethanol; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-1991-26390

Reference yield:

: 33617-49-1
diethyl <3,5-bis(benzyloxy)benzyl>phosphonate

: 70610-11-6
3,5-dihydroxy-4-(3-methyl-2-butenyl)-bibenzyl

Guidance literature:: Multi-step reaction with 5 steps

1: NaOMe / dimethylformamide / 0.5 h / 80 °C

2: 98 percent / H₂ / 5percent Pd/C / ethyl acetate / 3 h / 20 °C / 3750.3 Torr

3: 1) NaH / 1) DMF, 20 deg C 2) 20 deg C, 1 h

4: 1) BuLi / 1) THF, hexane, 3 h, reflux 2) 12 h, reflux

5: 90 percent / 3percent HCl / ethanol / 12 h / 20 °C

With hydrogenchloride; n-butyllithium; hydrogen; sodium methylate; sodium hydride; palladium on activated charcoal; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1055/s-1991-26390