(E)-3-(2,2,6,6-Tetramethyl-4-oxo-1-piperidinyl)-2-propenoic acid methyl ester

Base Information

• Chemical Name: (E)-3-(2,2,6,6-Tetramethyl-4-oxo-1-piperidinyl)-2-propenoic acid methyl ester
• CAS No.: 110998-13-5
• Molecular Formula: C13H21 N O3
• Molecular Weight: 239.3107
• Wikidata: Q76388947
• Mol file: 110998-13-5.mol

Synonyms:BRN 5534878;110998-13-5;(E)-3-(2,2,6,6-Tetramethyl-4-oxo-1-piperidinyl)-2-propenoic acid methyl ester;trans-N-beta-(2,2,6,6-Tetramethyl-4-oxo-1-piperidyl)acrylic acid methyl ester;2-Propenoic acid, 3-(2,2,6,6-tetramethyl-4-oxo-1-piperidinyl)-, methyl ester, (E)-;LS-123771

Chemical Property of (E)-3-(2,2,6,6-Tetramethyl-4-oxo-1-piperidinyl)-2-propenoic acid methyl ester

Chemical Property:

• Vapor Pressure: 0.000282mmHg at 25°C
• Boiling Point: 322.3°Cat760mmHg
• Flash Point: 148.7°C
• Density: 1.055g/cm³
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 239.15214353
• Heavy Atom Count: 17
• Complexity: 336

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CC(=O)CC(N1C=CC(=O)OC)(C)C)C
• Isomeric SMILES: CC1(CC(=O)CC(N1/C=C/C(=O)OC)(C)C)C

Technology Process of (E)-3-(2,2,6,6-Tetramethyl-4-oxo-1-piperidinyl)-2-propenoic acid methyl ester

There total 1 articles about (E)-3-(2,2,6,6-Tetramethyl-4-oxo-1-piperidinyl)-2-propenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2,2,6,6-Tetramethyl-4-piperidone (826-36-8) + propynoic acid methyl ester (922-67-8) → (E)-1-methoxycarbonyl-2-ethylene (110998-13-5)

Guidance literature:

In dichloromethane; for 2h; Ambient temperature;

DOI:10.1080/00397919608004784

upstream raw materials:

2,2,6,6-Tetramethyl-4-piperidone

propynoic acid methyl ester