1,3-dibromo-2-(2,6-dibromophenyl)benzene

Base Information

Chemical Name:1,3-dibromo-2-(2,6-dibromophenyl)benzene
CAS No.:97038-96-5
Molecular Formula:C12H6 Br4
Molecular Weight:469.796
Hs Code.:2903999090
Mol file:97038-96-5.mol

Synonyms:Biphenyl,2,2',6,6'-tetrabromo- (6CI); 2,2',6,6'-Tetrabromo-1,1'-biphenyl;2,2',6,6'-Tetrabromobiphenyl; PBB 54

Suppliers and Price of 1,3-dibromo-2-(2,6-dibromophenyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,2'',6,6''-Tetrabromo-1,1''-biphenyl
250mg
$ 495.00

Total 56 raw suppliers

Chemical Property of 1,3-dibromo-2-(2,6-dibromophenyl)benzene

Chemical Property:

Melting Point:215 °C(Solv: ethanol (64-17-5); ethyl ether (60-29-7))
Boiling Point:391.3°Cat760mmHg
Flash Point:184.8°C
PSA：0.00000
Density:2.14g/cm³
LogP:6.40360

Purity/Quality:

99% ^*data from raw suppliers

2,2'',6,6''-Tetrabromo-1,1''-biphenyl ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 2,2'',6,6''-Tetrabromo-1,1''-biphenyl is a research intermediate used in the preparation of triphenylenes, tetraphenylenes, and other related compound.

Technology Process of 1,3-dibromo-2-(2,6-dibromophenyl)benzene

There total 7 articles about 1,3-dibromo-2-(2,6-dibromophenyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 19821-80-8
1,3-dibromo-2-iodo-benzene

: 97038-96-5
2,2’,6,6’-tetrabromobiphenyl

Guidance literature:: 1,3-dibromo-2-iodo-benzene; With n-butyllithium; copper(ll) bromide; In diethyl ether; hexane; at -78 ℃; for 0.75h; Inert atmosphere; Schlenk technique;

With nitrobenzene; In diethyl ether; hexane; at -78 - 20 ℃; for 6h;

Reference yield: 60.0%

: 108-36-1
1,3-dibromobenzene

: 97038-96-5
2,2’,6,6’-tetrabromobiphenyl

Guidance literature:: 1,3-dibromobenzene; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

With copper(I) cyanide lithium chloride; p-benzoquinone; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201000517

Reference yield:

: 19821-80-8
1,3-dibromo-2-iodo-benzene

: 19230-27-4
2-chloro-1,3-dibromobenzene

: 97038-96-5
2,2’,6,6’-tetrabromobiphenyl

Guidance literature:: With n-butyllithium; copper dichloride; Multistep reaction. Yields of byproduct given; 1.) ether, hexane, -78 deg C, 2 h, 2.) ether, hexane, from -78 deg C to RT, 12 h;
DOI:10.1021/ja961065y