Mesitylhydrazine

Base Information

• Chemical Name: Mesitylhydrazine
• CAS No.: 13636-54-9
• Molecular Formula: C9H14 N2
• Molecular Weight: 150.224
• Hs Code.: 2928000090
• DSSTox Substance ID: DTXSID00352839
• Wikidata: Q82130228
• Mol file: 13636-54-9.mol

Synonyms:mesitylhydrazine;13636-54-9;(2,4,6-trimethylphenyl)hydrazine;SCHEMBL3212255;DTXSID00352839;BBL020465;STK893175;(2,4,6-Trimethyl-phenyl)-hydrazine;AKOS000200817;BB 0249761;EN300-07035

Chemical Property of Mesitylhydrazine

Chemical Property:

• Vapor Pressure: 0.0797mmHg at 25°C
• Melting Point: 60-61 °C
• Boiling Point: 226.9°Cat760mmHg
• PKA: 5?+-.0.33(Predicted)
• Flash Point: 103.6°C
• PSA: 38.05000
• Density: 1.036g/cm³
• LogP: 2.67070
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 150.115698455
• Heavy Atom Count: 11
• Complexity: 113

Purity/Quality:

98%Min ^*data from raw suppliers

MesitylhydrazineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1)C)NN)C

Technology Process of Mesitylhydrazine

There total 7 articles about Mesitylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C19H30N2O4 → 2,4,6-trimethylphenylhydrazine (13636-54-9)

Guidance literature:

With water; sodium hydroxide; In diethyl ether; at -10 ℃;

DOI:10.1039/c0cc02456b

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + 2,4,6-trimethylphenyl diazonium chloride (70335-45-4) → 2,4,6-trimethylphenylhydrazine (13636-54-9) + 1,3,5-trimethyl-benzene (108-67-8)

Guidance literature:

Reference yield:

N,N'-dicarbethoxy-2,4,6-trimethylphenylhydrazine (74404-40-3) → 2,4,6-trimethylphenylhydrazine (13636-54-9)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/ja01514a065

upstream raw materials:

N,N'-dicarbethoxy-2,4,6-trimethylphenylhydrazine

hydrogenchloride

2,4,6-trimethylphenyl diazonium chloride

1,3,5-trimethyl-benzene

Downstream raw materials:

3-pentanone 2,4,6-trimethylphenylhydrazone

6-(2-amino-3,4,5-trimethyl-phenyl)-6-oxo-hexanoic acid

5-amino-4-carboxamido-3-(methylthio)-1-(2,4,6-trimethylphenyl)pyrazole

(S)-5-[hydroxy(diphenyl)methyl]-2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c]-1,2,4-triazol-2-ium tetrafluoroborate