cis-Fecapentaene 12

Base Information

Chemical Name:cis-Fecapentaene 12
CAS No.:89300-15-2
Molecular Formula:C15H22O3
Molecular Weight:250.338
Hs Code.:
DSSTox Substance ID:DTXSID301034025

Synonyms:cis-Fecapentaene 12;CCRIS 3997;NIOSH/TY6395100;89300-15-2;TY63951000;(all-Z)-3-(1,3,5,7,9-Dodecapentaenyloxy)-1,2-propanediol;(all E)-(+-)-3-(1,3,5,7,9-Dodecapentaenyloxy)-1,2-propanediol;1,2-Propanediol, 3-(1,3,5,7,9-dodecapentaenyloxy)-, (all-Z)-;DTXSID301034025;LS-190749;3-(1,3,5,7,9-Dodecapentaenyloxy)-1,2-propanediol;(ALL E)-(+/-)-3-(1,3,5,7,9-DODECAPENTAENYLOXY)-1,2-PROPANEDIOL

Suppliers and Price of cis-Fecapentaene 12

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of cis-Fecapentaene 12

Chemical Property:

Vapor Pressure:1.09E-09mmHg at 25°C
Boiling Point:442.5°Cat760mmHg
Flash Point:221.4°C
Density:1.017g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:250.15689456
Heavy Atom Count:18
Complexity:312

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC=CC=CC=CC=CC=COCC(CO)O
Isomeric SMILES:CC/C=C\C=C/C=C\C=C/C=C\OCC(CO)O

Technology Process of cis-Fecapentaene 12

There total 22 articles about cis-Fecapentaene 12 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4313-03-5
(2E,4E)-hepta-2,4-dienal

: 89300-15-2,83248-46-8
all-trans-3-(dodeca-1,3,5,7,9-pentaenyloxy)propane-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) p-toluenesulfonic acid / 1.) THF; 2.) H₂O-THF

2: 2.) KOtBu / 1.) THF, -78 deg C; 2.) THF, -20 deg C

3: (CH₃)4NF*3H₂O / tetrahydrofuran / 0 °C

With potassium tert-butylate; tetramethylammonium fluoride; toluene-4-sulfonic acid; In tetrahydrofuran;

Reference yield:

: 89229-61-8
<(2,3-bis<(tert-butyldimethylsilyl)oxy>-propyl)oxy>dodeca-1,3,5,7,9-pentaene

: 89300-15-2,83248-46-8
all-trans-3-(dodeca-1,3,5,7,9-pentaenyloxy)propane-1,2-diol

Guidance literature:: With 6,6'-di-tert-butyl-4,4'-thiodi-o-cresol; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 1h; Yield given;

Reference yield:

: 100683-51-0
(E,E)-4,6-Nonadien-1-yn-3-ol

: 89300-15-2,83248-46-8
all-trans-3-(dodeca-1,3,5,7,9-pentaenyloxy)propane-1,2-diol

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / HCl

2: 1.)LiN(Si(CH₃)3)2 / 1.) THF, -78 deg C then 0 deg C; 2.) THF, -78 deg C then -30 deg C

3: LiAlH₄ / tetrahydrofuran / 2.5 h / Ambient temperature

4: tetrabutylammonium fluoride / tetrahydrofuran; diethyl ether / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00266a057