1-(5-Amino-2-methoxyphenyl)ethanone

Base Information

Chemical Name:1-(5-Amino-2-methoxyphenyl)ethanone
CAS No.:85276-70-6
Molecular Formula:C9H11NO2
Molecular Weight:165.192
Hs Code.:2922509090
DSSTox Substance ID:DTXSID40574790
Wikidata:Q82463958
Mol file:85276-70-6.mol

Synonyms:85276-70-6;1-(5-AMINO-2-METHOXYPHENYL)ETHANONE;Ethanone, 1-(5-amino-2-methoxyphenyl)- (9CI);1-(5-Amino-2-methoxyphenyl)ethan-1-one;SCHEMBL3884423;DTXSID40574790;AIDRUCBIROYFNK-UHFFFAOYSA-N;AKOS006330881;1-(5-amino-2-methoxy-phenyl)-ethanone

Suppliers and Price of 1-(5-Amino-2-methoxyphenyl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemcia Scientific
1-(5-Amino-2-methoxy-phenyl)-ethanone 95%
0.5 G
$ 345.00

American Custom Chemicals Corporation
1-(5-AMINO-2-METHOXYPHENYL)ETHANONE 95.00%
5MG
$ 500.12

Alichem
5'-Amino-2'-methoxyacetophenone
1g
$ 1519.80

Alichem
5'-Amino-2'-methoxyacetophenone
500mg
$ 782.40

Alichem
5'-Amino-2'-methoxyacetophenone
250mg
$ 499.20

AHH
1-(5-amino-2-methoxyphenyl)ethanone 97%
25g
$ 4005.00

Total 4 raw suppliers

Chemical Property of 1-(5-Amino-2-methoxyphenyl)ethanone

Chemical Property:

Melting Point:91°C
PSA：52.32000
LogP:2.06120
XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:165.078978594
Heavy Atom Count:12
Complexity:170

Purity/Quality:

99% ^*data from raw suppliers

1-(5-Amino-2-methoxy-phenyl)-ethanone 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=C(C=CC(=C1)N)OC

Technology Process of 1-(5-Amino-2-methoxyphenyl)ethanone

There total 7 articles about 1-(5-Amino-2-methoxyphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 51410-09-4
acetic acid-(3-acetyl-4-methoxy-anilide)

: 85276-70-6
5'-amino-2'-methoxyacetophenone

Guidance literature:: With hydrogenchloride; In ethanol; water;

Reference yield:

: 2516-96-3
2-chloro-5-nitrobenzoic acid

: 85276-70-6
5'-amino-2'-methoxyacetophenone

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol / 12 h / Heating / reflux

1.2: 0.5 h / 20 °C / pH ~ 2

2.1: thionyl chloride / 4 h / Heating / reflux

3.1: triethylamine; magnesium chloride / toluene / 1 h / 0 - 20 °C

3.2: 0.5 h / 0 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol

With thionyl chloride; hydrogen; triethylamine; magnesium chloride; palladium 10% on activated carbon; In methanol; toluene;

Reference yield:

: 40751-89-1
2-methoxy-5-nitrobenzoic acid

: 85276-70-6
5'-amino-2'-methoxyacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 4 h / Heating / reflux

2.1: triethylamine; magnesium chloride / toluene / 1 h / 0 - 20 °C

2.2: 0.5 h / 0 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol

With thionyl chloride; hydrogen; triethylamine; magnesium chloride; palladium 10% on activated carbon; In methanol; toluene;