Benzenemethanol, 4-(1-methylsilacyclobut-1-yl)-

Base Information

Chemical Name:Benzenemethanol, 4-(1-methylsilacyclobut-1-yl)-
CAS No.:853654-20-3
Molecular Formula:C11H16OSi
Molecular Weight:192.333
Hs Code.:
DSSTox Substance ID:DTXSID70467222
Nikkaji Number:J2.165.077C
Wikidata:Q82294034

Synonyms:853654-20-3;Benzenemethanol, 4-(1-methylsilacyclobut-1-yl)-;SCHEMBL15382351;DTXSID70467222;4-(1-Methylsilacyclobutane-1-yl)benzyl alcohol

Suppliers and Price of Benzenemethanol, 4-(1-methylsilacyclobut-1-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanol, 4-(1-methylsilacyclobut-1-yl)-

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:192.097041664
Heavy Atom Count:13
Complexity:169

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si]1(CCC1)C2=CC=C(C=C2)CO

Technology Process of Benzenemethanol, 4-(1-methylsilacyclobut-1-yl)-

There total 5 articles about Benzenemethanol, 4-(1-methylsilacyclobut-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 873292-81-0
4-(1-methyl-siletan-1-yl)-benzaldehyde

: 853654-20-3
[4-(1-methyl-siletan-1-yl)-phenyl]-methanol

Guidance literature:: With diisobutylaluminium hydride;
DOI:10.1055/s-0029-1219531

Reference yield: 94.0%

: 853654-19-0
1-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenyl]-1-methyl-siletane

: 853654-20-3
[4-(1-methyl-siletan-1-yl)-phenyl]-methanol

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2005.03.110

Reference yield:

: 873292-73-0
4-(1-methylsilethanyl)benzaldehyde dimethyl acetal

: 853654-20-3
[4-(1-methyl-siletan-1-yl)-phenyl]-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent Spectr_. / aq. HCl / diethyl ether / 5 h

2: 87 percent / DIBAL-H / CH₂Cl₂ / 2 h / -78 - 20 °C

With hydrogenchloride; diisobutylaluminium hydride; In diethyl ether; dichloromethane;
DOI:10.1021/jo052015r