Benzaldehyde, 2-bromo-3,6-dimethoxy-

Base Information

• Chemical Name: Benzaldehyde, 2-bromo-3,6-dimethoxy-
• CAS No.: 85432-87-7
• Molecular Formula: C9H9BrO3
• Molecular Weight: 245.073
• DSSTox Substance ID: DTXSID80463437
• Nikkaji Number: J1.875.829F
• Wikidata: Q82288314
• Mol file: 85432-87-7.mol

Synonyms:2-Bromo-3,6-dimethoxybenzaldehyde;Benzaldehyde, 2-bromo-3,6-dimethoxy-;85432-87-7;SCHEMBL4941209;DTXSID80463437

Chemical Property of Benzaldehyde, 2-bromo-3,6-dimethoxy-

Chemical Property:

• XLogP3: 2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 243.97351
• Heavy Atom Count: 13
• Complexity: 174

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C(=C(C=C1)OC)Br)C=O

Technology Process of Benzaldehyde, 2-bromo-3,6-dimethoxy-

There total 14 articles about Benzaldehyde, 2-bromo-3,6-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(2'-bromo-3',6'-dimethoxyphenyl)-1,3-dioxane (311312-60-4) → 2-bromo-3,6-dimethoxybenzaldehyde (85432-87-7)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; for 0.166667h;

DOI:10.1021/ja005552w

Reference yield: 100.0%

2-(2-bromo-3,6-dimethoxy-phenyl)-[1,3]dioxolane → 2-bromo-3,6-dimethoxybenzaldehyde (85432-87-7)

Guidance literature:

With hydrogenchloride; at 0 ℃; for 0.5h;

DOI:10.1021/jo051444m

Reference yield: 95.0%

(2-bromo-3,6-dimethoxyphenyl)methanol (327164-05-6) → 2-bromo-3,6-dimethoxybenzaldehyde (85432-87-7)

Guidance literature:

With 4 A molecular sieve; pyridinium chlorochromate; In dichloromethane; for 10h;

DOI:10.1021/jo001523s

upstream raw materials:

2,5-dimethoxybenzaldehyde

bromine

acetic acid

(2-bromo-3,6-dimethoxyphenyl)methanol

Downstream raw materials:

2-bromo-3,6-dimethoxybenzoyl bromide

2-bromo-3-hydroxy-6-methoxybenzaldehyde

rac-1-(2-bromo-3,6-dimethoxyphenyl)prop-2-en-1-ol

2-bromo-3,6-dimethoxy-5-(2-propenyl)benzaldehyde