1-Piperidinecarboxylic acid, 2-(hydroxymethyl)-3,4,5-tris(phenylmethoxy)-6-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3S,4R,5S,6R)-

Base Information

Chemical Name:1-Piperidinecarboxylic acid, 2-(hydroxymethyl)-3,4,5-tris(phenylmethoxy)-6-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3S,4R,5S,6R)-
CAS No.:856174-72-6
Molecular Formula:C43H45NO7
Molecular Weight:687.833
Hs Code.:

1-Piperidinecarboxylic acid,
2-(hydroxymethyl)-3,4,5-tris(phenylmethoxy)-6-[(phenylmethoxy)methyl]-,
phenylmethyl ester, (2R,3S,4R,5S,6R)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Piperidinecarboxylic acid, 2-(hydroxymethyl)-3,4,5-tris(phenylmethoxy)-6-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3S,4R,5S,6R)-

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Technology Process of 1-Piperidinecarboxylic acid, 2-(hydroxymethyl)-3,4,5-tris(phenylmethoxy)-6-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3S,4R,5S,6R)-

There total 1 articles about 1-Piperidinecarboxylic acid, 2-(hydroxymethyl)-3,4,5-tris(phenylmethoxy)-6-[(phenylmethoxy)methyl]-, phenylmethyl ester, (2R,3S,4R,5S,6R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 3,4,5,7-tetra-O-benzyl-6-[(benzyloxycarbonyl)amino]-1,2,6-trideoxyhept-1-enitol

: 856174-72-6
1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-(benzyloxycarbonyl)imino-D-glycero-L-galacto-heptitol

: 856174-73-7
1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-(benzyloxycarbonyl)imino-L-glycero-L-gluco-heptitol

: 1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-(benzyloxycarbonyl)imino-D-glycero-L-gluco-heptitol

Guidance literature:: 3,4,5,7-tetra-O-benzyl-6-[(benzyloxycarbonyl)amino]-1,2,6-trideoxyhept-1-enitol; With mercury(II) diacetate; In tetrahydrofuran; for 35h; Heating;

With potassium chloride; In chloroform; at 20 ℃; for 4h;

With sodium tetrahydroborate; oxygen; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/jm050169t

Reference yield: 99.0%

: 856174-72-6
1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-(benzyloxycarbonyl)imino-D-glycero-L-galacto-heptitol

: 856003-84-4
(2,3,4,6-tetra-O-benzyl-N-benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glycero-D-galacto-heptitolyl)aldehyde

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In dichloromethane; at 20 ℃;
DOI:10.1002/cjoc.201600862