2-hydroxy-1-naphthalaldehyde salicyloylhydrazone

Base Information

• Chemical Name: 2-hydroxy-1-naphthalaldehyde salicyloylhydrazone
• CAS No.: 54009-54-0
• Molecular Formula: C18H14 N2 O3
• Molecular Weight: 306.321
• Hs Code.: 2928000090
• Mol file: 54009-54-0.mol

Synonyms:Benzoicacid, 2-hydroxy-, [(2-hydroxy-1-naphthalenyl)methylene]hydrazide (9CI); 2-Hydroxy-1-naphthaldehydesalicylhydrazone; 2-Hydroxy-1-naphthaldehyde salicylic acid hydrazone; ZLIII109A

Chemical Property of 2-hydroxy-1-naphthalaldehyde salicyloylhydrazone

Chemical Property:

• Boiling Point: 526.2°Cat760mmHg
• PKA: 7.85±0.50(Predicted)
• Flash Point: 272.1°C
• PSA: 81.92000
• Density: 1.4g/cm³
• LogP: 3.22930

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-hydroxy-1-naphthalaldehyde salicyloylhydrazone

There total 3 articles about 2-hydroxy-1-naphthalaldehyde salicyloylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.8%

2-Hydroxybenzoylhydrazine (936-02-7) + 2-hydroxynaphthalene-1-carbaldehyde (708-06-5) → 2-hydroxy-N'-((2-hydroxy-naphthalen-1-yl)methylene)benzohydrazide (54009-54-0)

Guidance literature:

With zinc(II) perchlorate; In methanol; at 20 ℃; for 3h;

DOI:10.1002/bio.4025

Reference yield:

C18H13N2O3(1-)*Al(3+) → 2-hydroxy-N'-((2-hydroxy-naphthalen-1-yl)methylene)benzohydrazide (54009-54-0)

Guidance literature:

With disodium ethylenediamine tetraacetic acid;

DOI:10.1039/d0ra02101f

Reference yield:

C18H13N2O3(1-)*Mg(2+) → 2-hydroxy-N'-((2-hydroxy-naphthalen-1-yl)methylene)benzohydrazide (54009-54-0)

Guidance literature:

With disodium ethylenediamine tetraacetic acid;

DOI:10.1039/d0ra02101f

upstream raw materials:

2-Hydroxybenzoylhydrazine

2-hydroxynaphthalene-1-carbaldehyde

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