Phenylmethyl 2-hydroxy-1-naphthalenecarboxylate

Base Information

Chemical Name:Phenylmethyl 2-hydroxy-1-naphthalenecarboxylate
CAS No.:86170-47-0
Molecular Formula:C18H14O3
Molecular Weight:278.307
Hs Code.:
DSSTox Substance ID:DTXSID80478349

Synonyms:phenylmethyl 2-hydroxy-1-naphthalenecarboxylate;86170-47-0;SCHEMBL7392898;DTXSID80478349;LHFVUEILYKNBNJ-UHFFFAOYSA-N

Suppliers and Price of Phenylmethyl 2-hydroxy-1-naphthalenecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenylmethyl 2-hydroxy-1-naphthalenecarboxylate

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:278.094294304
Heavy Atom Count:21
Complexity:348

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC(=O)C2=C(C=CC3=CC=CC=C32)O

Technology Process of Phenylmethyl 2-hydroxy-1-naphthalenecarboxylate

There total 1 articles about Phenylmethyl 2-hydroxy-1-naphthalenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 100-39-0
benzyl bromide

: 2283-08-1
2-hydroxy-1-naphthalenecarboxylic acid

: 86170-47-0
2-hydroxynaphthalene-1-carboxylic acid benzyl ester

Guidance literature:: With potassium hydrogencarbonate; In N,N-dimethyl-formamide; at 40 ℃;
DOI:10.1081/SCC-200046532

Reference yield: 95.0%

: 86170-47-0
2-hydroxynaphthalene-1-carboxylic acid benzyl ester

: benzyl (R)-1-bromo-2-oxo-1,2-dihydronaphthalene-1-carboxylate

Guidance literature:: With 2-[(4S,5S)-4,5-dihydro-4,5-diphenyl-2-oxazolyl]-N-[2-[(4S,5S)-4,5-dihydro-4,5-diphenyl-2-oxazolyl]phenyl]benzenamine; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at -45 ℃; for 0.5h; enantioselective reaction;
DOI:10.1002/adsc.201800067

Reference yield: 81.0%

: 86170-47-0
2-hydroxynaphthalene-1-carboxylic acid benzyl ester

: benzyl 1-azido-2-oxo-1,2-dihydronaphthalene-1-carboxylate

Guidance literature:: With tert.-butylhydroperoxide; trimethylsilylazide; copper(I) bromide; In water; acetonitrile; at 20 ℃;
DOI:10.1039/c6cc04894c