2H-3,1-Benzoxazin-2-one, 1-[3-[[2-[3,4-dihydro-3-oxo-6-(phenylmethoxy)-2H-1,4-benzoxazin-8-yl]- 2-hydroxyethyl]amino]-3-methylbutyl]-1,4-dihydro-, mono(trifluoroacetate) (salt)

Base Information

Chemical Name:2H-3,1-Benzoxazin-2-one, 1-[3-[[2-[3,4-dihydro-3-oxo-6-(phenylmethoxy)-2H-1,4-benzoxazin-8-yl]- 2-hydroxyethyl]amino]-3-methylbutyl]-1,4-dihydro-, mono(trifluoroacetate) (salt)
CAS No.:861841-77-2
Molecular Formula:C30H33N3O6.C2HF3O2
Molecular Weight:645.632
Hs Code.:

2H-3,1-Benzoxazin-2-one,
1-[3-[[2-[3,4-dihydro-3-oxo-6-(phenylmethoxy)-2H-1,4-benzoxazin-8-yl]-
2-hydroxyethyl]amino]-3-methylbutyl]-1,4-dihydro-,
mono(trifluoroacetate) (salt)

Synonyms:

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Chemical Property of 2H-3,1-Benzoxazin-2-one, 1-[3-[[2-[3,4-dihydro-3-oxo-6-(phenylmethoxy)-2H-1,4-benzoxazin-8-yl]- 2-hydroxyethyl]amino]-3-methylbutyl]-1,4-dihydro-, mono(trifluoroacetate) (salt)

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MSDS Files:: SDS file from LookChem

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Technology Process of 2H-3,1-Benzoxazin-2-one, 1-[3-[[2-[3,4-dihydro-3-oxo-6-(phenylmethoxy)-2H-1,4-benzoxazin-8-yl]- 2-hydroxyethyl]amino]-3-methylbutyl]-1,4-dihydro-, mono(trifluoroacetate) (salt)

There total 3 articles about 2H-3,1-Benzoxazin-2-one, 1-[3-[[2-[3,4-dihydro-3-oxo-6-(phenylmethoxy)-2H-1,4-benzoxazin-8-yl]- 2-hydroxyethyl]amino]-3-methylbutyl]-1,4-dihydro-, mono(trifluoroacetate) (salt) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 861871-26-3
1-(3-amino-3-methyl-butyl)-1,4-dihydro-benzo[d][1,3]oxazin-2-one

: 76-05-1
trifluoroacetic acid

: 861841-77-2
1-{3-[2-(6-benzyloxy-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-8-yl)-2-hydroxy-ethylamino]-3-methyl-butyl}-1,4-dihydro-benzo[d][1,3]oxazin-2-one trifluoroacetate

Guidance literature:: 1-(3-amino-3-methyl-butyl)-1,4-dihydro-benzo[d][1,3]oxazin-2-one; 8-(2-hydroxy-2-ethoxyacetyl)-6-(phenylmethoxy)-4H-1,4-benzoxazin-3-one; In tetrahydrofuran; at 60 ℃; for 0.25h;

With lithium borohydride; In tetrahydrofuran; dichloromethane; water; at 0 ℃; for 1.25h;

trifluoroacetic acid; In water; acetonitrile;

Reference yield: 30.0%

: 861871-26-3
1-(3-amino-3-methyl-butyl)-1,4-dihydro-benzo[d][1,3]oxazin-2-one

: 124955-27-7
8-(2-hydroxy-2-ethoxyacetyl)-6-(phenylmethoxy)-4H-1,4-benzoxazin-3-one

: 861841-77-2
1-{3-[2-(6-benzyloxy-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-8-yl)-2-hydroxy-ethylamino]-3-methyl-butyl}-1,4-dihydro-benzo[d][1,3]oxazin-2-one trifluoroacetate

Guidance literature:: 1-(3-amino-3-methyl-butyl)-1,4-dihydro-benzo[d][1,3]oxazin-2-one; 8-(2-hydroxy-2-ethoxyacetyl)-6-(phenylmethoxy)-4H-1,4-benzoxazin-3-one; In tetrahydrofuran; at 60 ℃; for 0.25h;

With lithium borohydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

With water; In tetrahydrofuran; dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 861841-76-1
1-{3-[2-(6-benzyloxy-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-8-yl)-2-hydroxy-ethylamino]-3-methyl-butyl}-1,4-dihydro-benzo[1,3]oxazin-2-one

: 76-05-1
trifluoroacetic acid

: 861841-77-2
1-{3-[2-(6-benzyloxy-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-8-yl)-2-hydroxy-ethylamino]-3-methyl-butyl}-1,4-dihydro-benzo[d][1,3]oxazin-2-one trifluoroacetate

Guidance literature:: 1-{3-[2-(6-benzyloxy-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-8-yl)-2-hydroxy-ethylamino]-3-methyl-butyl}-1,4-dihydro-benzo[1,3]oxazin-2-one; trifluoroacetic acid; In tetrahydrofuran; at 0 - 60 ℃; for 0.25h;

With lithium borohydride; In tetrahydrofuran; dichloromethane; at 0 ℃; for 0.25h;