5-Norbornene-2,3-dicarboximide, 5-(alpha-hydroxy-2-pyridylbenzyl)-N-methyl-7-(alpha-2-pyridylbenzylidene)-, endo-

Base Information

Chemical Name:5-Norbornene-2,3-dicarboximide, 5-(alpha-hydroxy-2-pyridylbenzyl)-N-methyl-7-(alpha-2-pyridylbenzylidene)-, endo-
CAS No.:1740-11-0
Molecular Formula:C₃₄H₂₇N₃O₃
Molecular Weight:525.607
Hs Code.:
DSSTox Substance ID:DTXSID60938451

Synonyms:1740-11-0;BRN 0871634;5-Norbornene-2,3-dicarboximide, 5-(alpha-hydroxy-2-pyridylbenzyl)-N-methyl-7-(alpha-2-pyridylbenzylidene)-, endo-;SCHEMBL16406509;DTXSID60938451;5-[Hydroxy(phenyl)(pyridin-2-yl)methyl]-2-methyl-8-[phenyl(pyridin-2-yl)methylidene]-3a,4,7,7a-tetrahydro-1H-4,7-methanoisoindole-1,3(2H)-dione

Suppliers and Price of 5-Norbornene-2,3-dicarboximide, 5-(alpha-hydroxy-2-pyridylbenzyl)-N-methyl-7-(alpha-2-pyridylbenzylidene)-, endo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Norbornene-2,3-dicarboximide, 5-(alpha-hydroxy-2-pyridylbenzyl)-N-methyl-7-(alpha-2-pyridylbenzylidene)-, endo-

Chemical Property:

Vapor Pressure:2.08E-24mmHg at 25°C
Boiling Point:762°Cat760mmHg
Flash Point:414.6°C
Density:1.329g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:525.20524173
Heavy Atom Count:40
Complexity:1070

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C(=O)C2C3C=C(C(C2C1=O)C3=C(C4=CC=CC=C4)C5=CC=CC=N5)C(C6=CC=CC=C6)(C7=CC=CC=N7)O

Technology Process of 5-Norbornene-2,3-dicarboximide, 5-(alpha-hydroxy-2-pyridylbenzyl)-N-methyl-7-(alpha-2-pyridylbenzylidene)-, endo-

There total 1 articles about 5-Norbornene-2,3-dicarboximide, 5-(alpha-hydroxy-2-pyridylbenzyl)-N-methyl-7-(alpha-2-pyridylbenzylidene)-, endo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 991-42-4,5779-10-2,5779-11-3,5779-12-4,5779-37-3,5784-49-6,5784-50-9,5784-51-0,5818-01-9
[5-(α-hydroxy-α-2-pyridylbenzyl)-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide]

: 74-88-4
methyl iodide

: 6434-24-8,1740-11-0
5-(α-hydroxy-α-2-pyridylbenzyl)-N-methyl-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1016/j.bmc.2012.05.014

Reference yield: 51.0%

: chloromethyl diphenylacetate

: 6434-24-8,1740-11-0
5-(α-hydroxy-α-2-pyridylbenzyl)-N-methyl-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide

: 5-(α-hydroxy-α-2-pyridylbenzyl)-N-methyl-7-[α-2-pyridyl-N-(diphenylacetoyloxymethyl)benzylidene]-5-norbornene-2,3-dicarboximide iodide

Guidance literature:: chloromethyl diphenylacetate; With sodium iodide; In acetone; at 20 ℃; for 3h;

5-(α-hydroxy-α-2-pyridylbenzyl)-N-methyl-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide; In acetonitrile; at 80 ℃; for 16h;
DOI:10.1016/j.bmc.2012.05.014

Reference yield: 37.0%

: 5335-05-7
chloromethyl benzoate

: 6434-24-8,1740-11-0
5-(α-hydroxy-α-2-pyridylbenzyl)-N-methyl-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide

: 5-(α-hydroxy-α-2-pyridylbenzyl)-N-methyl-7-[α-2-pyridyl-N-(benzoyloxymethyl)benzylidene]-5-norbornene-2,3-dicarboximide iodide

Guidance literature:: chloromethyl benzoate; With sodium iodide; In acetone; at 20 ℃; for 0.5h;

5-(α-hydroxy-α-2-pyridylbenzyl)-N-methyl-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide; In acetonitrile; at 80 ℃; for 16h;
DOI:10.1016/j.bmc.2012.05.014