2,5,9,11-Tetramethyl-5H-quinindoline

Base Information

Chemical Name:2,5,9,11-Tetramethyl-5H-quinindoline
CAS No.:158470-95-2
Molecular Formula:C₁₉H₁₈N₂
Molecular Weight:274.365
Hs Code.:
DSSTox Substance ID:DTXSID00935924
Nikkaji Number:J626.299F
Wikidata:Q82912030
ChEMBL ID:CHEMBL119536

Synonyms:2,5,9,11-Tetramethyl-5H-quinindoline;CCRIS 7307;158470-95-2;5H-Quinindoline, 2,5,9,11-tetramethyl-;2,5,9,11-Tetramethyl-5H-indolo[2,3-b]quinoline;CHEMBL119536;DTXSID00935924

Suppliers and Price of 2,5,9,11-Tetramethyl-5H-quinindoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2,5,9,11-Tetramethyl-5H-quinindoline

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:436.552°C at 760 mmHg
Flash Point:217.819°C
Density:1.16g/cm³
XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:274.146998583
Heavy Atom Count:21
Complexity:395

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)N=C3C2=C(C4=C(N3C)C=CC(=C4)C)C

Technology Process of 2,5,9,11-Tetramethyl-5H-quinindoline

There total 6 articles about 2,5,9,11-Tetramethyl-5H-quinindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3913-18-6
2-chloro-4,6-dimethylquinoline

: 158470-95-2
2,5,9,11-tetramethyl-5H-indolo<2,3-b>quinoline

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / 10 h / 150 - 160 °C

2: SnCl₂, 36percent aq. HCl / ethanol / 0.5 h / Heating

3: NaNO₂, aq. HCl / ethanol; H₂O / 5 - 10 °C

4: 18 percent / PPA / 130 - 180 °C

5: 2.) 20percent NaOH / 1.) toluene, 150 to 160 deg C, 12 h, 2.) H₂O

With hydrogenchloride; sodium hydroxide; tin(ll) chloride; sodium nitrite; In ethanol; water;
DOI:10.1021/jm00047a008

Reference yield:

: 1026008-36-5
N¹-(4,6-Dimethyl-quinolin-2-yl)-4-methyl-benzene-1,2-diamine

: 158470-95-2
2,5,9,11-tetramethyl-5H-indolo<2,3-b>quinoline

Guidance literature:: Multi-step reaction with 3 steps

1: NaNO₂, aq. HCl / ethanol; H₂O / 5 - 10 °C

2: 18 percent / PPA / 130 - 180 °C

3: 2.) 20percent NaOH / 1.) toluene, 150 to 160 deg C, 12 h, 2.) H₂O

With hydrogenchloride; sodium hydroxide; sodium nitrite; In ethanol; water;
DOI:10.1021/jm00047a008

Reference yield:

: 158470-92-9
4,6-dimethyl-2-(4-methyl-2-nitroanilino)quinoline

: 158470-95-2
2,5,9,11-tetramethyl-5H-indolo<2,3-b>quinoline

Guidance literature:: Multi-step reaction with 4 steps

1: SnCl₂, 36percent aq. HCl / ethanol / 0.5 h / Heating

2: NaNO₂, aq. HCl / ethanol; H₂O / 5 - 10 °C

3: 18 percent / PPA / 130 - 180 °C

4: 2.) 20percent NaOH / 1.) toluene, 150 to 160 deg C, 12 h, 2.) H₂O

With hydrogenchloride; sodium hydroxide; tin(ll) chloride; sodium nitrite; In ethanol; water;
DOI:10.1021/jm00047a008