N-[(4-Chlorophenyl)carbamothioyl]benzenesulfonamide

Base Information

Chemical Name:N-[(4-Chlorophenyl)carbamothioyl]benzenesulfonamide
CAS No.:70472-39-8
Molecular Formula:C13H11ClN2O2S2
Molecular Weight:326.8216
Hs Code.:
NSC Number:144071
DSSTox Substance ID:DTXSID40398190
ChEMBL ID:CHEMBL76000

Synonyms:70472-39-8;NSC144071;CHEMBL76000;DTXSID40398190;NSC-144071;N-[(4-Chlorophenyl)carbamothioyl]benzenesulfonamide

Suppliers and Price of N-[(4-Chlorophenyl)carbamothioyl]benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of N-[(4-Chlorophenyl)carbamothioyl]benzenesulfonamide

Chemical Property:

Vapor Pressure:5.58E-09mmHg at 25°C
Boiling Point:469.3°Cat760mmHg
Flash Point:237.6°C
Density:1.48g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:325.9950476
Heavy Atom Count:20
Complexity:422

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)S(=O)(=O)NC(=S)NC2=CC=C(C=C2)Cl

Technology Process of N-[(4-Chlorophenyl)carbamothioyl]benzenesulfonamide

There total 3 articles about N-[(4-Chlorophenyl)carbamothioyl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1424-53-9
benzenesulfonyl isothiocyanate

: 106-47-8
4-chloro-aniline

: 70472-39-8
N-(phenylsulfonyl)-N'-(4-chlorophenyl)thiourea

Guidance literature:: In benzene;

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 70472-39-8
N-(phenylsulfonyl)-N'-(4-chlorophenyl)thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 90.2 percent / liq. NH₃ / CH₂Cl₂ / 4 h / -78 °C

2: 1.) aq. NaOH / 1.) acetone, RT, 30 min, 2.) acetone, reflux, 4 h

With sodium hydroxide; ammonia; In dichloromethane;
DOI:10.1021/jm9607818

Reference yield:

: 98-10-2
benzenesulfonamide

: 2131-55-7
4-Chlorophenyl isothiocyanate

: 70472-39-8
N-(phenylsulfonyl)-N'-(4-chlorophenyl)thiourea

Guidance literature:: With sodium hydroxide; Yield given. Multistep reaction; 1.) acetone, RT, 30 min, 2.) acetone, reflux, 4 h;
DOI:10.1021/jm9607818