Methanesulfonic acid, trifluoro-, 3,3,5,5-tetramethyl-1-cyclohexen-1-yl ester

Base Information

Chemical Name:Methanesulfonic acid, trifluoro-, 3,3,5,5-tetramethyl-1-cyclohexen-1-yl ester
CAS No.:86544-77-6
Molecular Formula:C11H17F3O3S
Molecular Weight:286.315
Hs Code.:

Synonyms:3,3,5,5-tetramethylcyclohex-1-enyl trifluoromethanesulfonate;3,3,5,5-tetramethyl-1-cyclohexenyl trifluoromethanesulfonate;trifluoromethanesulfonic acid 3,3,5,5-tetramethylcyclohex-1-enyl ester;3,3,5,5-tetramethyl-cyclohex-1-en-1-yl trifluoromethanesulfonate;trifluoro-methanesulfonic acid 3,3,5,5-tetramethyl-cyclohex-1-enyl ester;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanesulfonic acid, trifluoro-, 3,3,5,5-tetramethyl-1-cyclohexen-1-yl ester

Chemical Property:

PSA：51.75000
LogP:4.66350

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanesulfonic acid, trifluoro-, 3,3,5,5-tetramethyl-1-cyclohexen-1-yl ester

There total 4 articles about Methanesulfonic acid, trifluoro-, 3,3,5,5-tetramethyl-1-cyclohexen-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 14376-79-5
3,3,5,5-tetramethylcyclohexanone

: 358-23-6
trifluoromethylsulfonic anhydride

: 86544-77-6
3,3,5,5-tetramethylcyclohex-1-enyl trifluoromethanesulfonate

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; for 7h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80412-9

Reference yield: 66.0%

: 86544-77-6
3,3,5,5-tetramethylcyclohex-1-enyl trifluoromethanesulfonate

Guidance literature:

Reference yield:

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 86544-77-6
3,3,5,5-tetramethylcyclohex-1-enyl trifluoromethanesulfonate

Guidance literature:: 3,3,5,5-tetramethylcyclohexanone; With lithium hexamethyldisilazane; In tetrahydrofuran; at -70 ℃; for 0.916667h; Cooling with acetone-dry ice;

N,N-phenylbistrifluoromethane-sulfonimide; In tetrahydrofuran; at -70 - 20 ℃; for 13.5h; Product distribution / selectivity; Cooling with acetone-dry ice;