9-Chloro-6-methylacridine-4-carbonyl chloride

Base Information

Chemical Name:9-Chloro-6-methylacridine-4-carbonyl chloride
CAS No.:86611-43-0
Molecular Formula:C15H9Cl2NO
Molecular Weight:290.149
Hs Code.:
DSSTox Substance ID:DTXSID50544641
Wikidata:Q82421826

Synonyms:9-CHLORO-6-METHYLACRIDINE-4-CARBONYL CHLORIDE;86611-43-0;DTXSID50544641

Suppliers and Price of 9-Chloro-6-methylacridine-4-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-Chloro-6-methylacridine-4-carbonyl chloride

Chemical Property:

XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:289.0061193
Heavy Atom Count:19
Complexity:362

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC2=NC3=C(C=CC=C3C(=O)Cl)C(=C2C=C1)Cl

Technology Process of 9-Chloro-6-methylacridine-4-carbonyl chloride

There total 1 articles about 9-Chloro-6-methylacridine-4-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7697-27-0
2-bromo-4-methylbenzoic acid

: 86611-43-0
9-Chloro-6-methyl-acridine-4-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / K₂CO₃, Cu, coprous oxide / 2-ethoxy-ethanol / 0.5 h / 120 °C

2: 41 percent / conc. H₂SO₄ / 2 h / 90 °C

3: SOCl₂, DMF / 1 h / Heating

With copper(I) oxide; thionyl chloride; sulfuric acid; copper; potassium carbonate; N,N-dimethyl-formamide; In 2-ethoxy-ethanol;
DOI:10.1021/jm00365a013

Reference yield:

: 86611-43-0
9-Chloro-6-methyl-acridine-4-carbonyl chloride

: 78847-60-6
9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂; H₂O

2: methanol / Heating

In methanol; dichloromethane; water;
DOI:10.1021/jm00365a013