9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride

Base Information

Chemical Name:9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride
CAS No.:78847-60-6
Molecular Formula:C₂₅H₂₅N₅O₅S*ClH
Molecular Weight:544.031
Hs Code.:

Synonyms:9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride

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Chemical Property of 9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride

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Technology Process of 9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride

There total 6 articles about 9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7697-27-0
2-bromo-4-methylbenzoic acid

: 78847-60-6
9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / K₂CO₃, Cu, coprous oxide / 2-ethoxy-ethanol / 0.5 h / 120 °C

2: 41 percent / conc. H₂SO₄ / 2 h / 90 °C

3: SOCl₂, DMF / 1 h / Heating

4: CH₂Cl₂; H₂O

5: methanol / Heating

With copper(I) oxide; thionyl chloride; sulfuric acid; copper; potassium carbonate; N,N-dimethyl-formamide; In methanol; 2-ethoxy-ethanol; dichloromethane; water;
DOI:10.1021/jm00365a013

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 78847-60-6
9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / K₂CO₃, Cu, coprous oxide / 2-ethoxy-ethanol / 0.5 h / 120 °C

2: 41 percent / conc. H₂SO₄ / 2 h / 90 °C

3: SOCl₂, DMF / 1 h / Heating

4: CH₂Cl₂; H₂O

5: methanol / Heating

With copper(I) oxide; thionyl chloride; sulfuric acid; copper; potassium carbonate; N,N-dimethyl-formamide; In methanol; 2-ethoxy-ethanol; dichloromethane; water;
DOI:10.1021/jm00365a013

Reference yield:

: 78847-67-3
3-methyl-5-carboxy-9(10H)-acridanone

: 78847-60-6
9-(4-Methanesulfonylamino-2-methoxy-phenylamino)-6-methyl-acridine-4-carboxylic acid carbamoylmethyl-amide; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂, DMF / 1 h / Heating

2: CH₂Cl₂; H₂O

3: methanol / Heating

With thionyl chloride; N,N-dimethyl-formamide; In methanol; dichloromethane; water;
DOI:10.1021/jm00365a013