Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-, methyl ester

Base Information

Chemical Name:Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-, methyl ester
CAS No.:868836-16-2
Molecular Formula:C42H61N3O7S2
Molecular Weight:826.175
Hs Code.:

Octanoic acid,
8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino]
butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-, methyl
ester

Synonyms:

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Chemical Property of Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-, methyl ester

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Technology Process of Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-, methyl ester

There total 5 articles about Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.3%

: 868836-13-9
1-amino-4-{N-[2,4,6-(trimethyl)benzenesulfonyl]}-8-{N-[4-(tert-butyl)benzyl]-N-[2,4,6-(trimethyl)benzenesulfonyl]}amino-4-azaoctane

: 41624-92-4
methyl 8-chloro-8-oxooctanoate

: 868836-16-2
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(4-tert-butyl)benzyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanoic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jm0505009

Reference yield: 78.3%

: 868836-16-2
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(4-tert-butyl)benzyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanoic acid methyl ester

Guidance literature:

Reference yield:

: C₃₃H₄₁N₃O₆S₂

: 868836-16-2
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(4-tert-butyl)benzyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0.5 h / 0 °C

1.2: 71.6 percent / dimethylformamide / 12 h

2.1: 70.8 percent / hydrazine / methanol / 12 h / Heating

3.1: 78.3 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With sodium hydride; triethylamine; hydrazine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0505009