Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-

Base Information

Chemical Name:Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-
CAS No.:868836-20-8
Molecular Formula:C41H59N3O7S2
Molecular Weight:812.148
Hs Code.:

Octanoic acid,
8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino]
butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-

Synonyms:

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Chemical Property of Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-

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Technology Process of Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo-

There total 6 articles about Octanoic acid, 8-[[3-[[4-[[(4-methylphenyl)methyl][(2,4,6-trimethylphenyl)sulfonyl]amino] butyl][(2,4,6-trimethylphenyl)sulfonyl]amino]propyl]amino]-8-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 868836-16-2
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(4-tert-butyl)benzyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanoic acid methyl ester

: 868836-20-8
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(4-tert-butyl)benzyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanoic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jm0505009

Reference yield: 80.0%

: 868836-20-8
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(4-tert-butyl)benzyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanoic acid

Guidance literature:

Reference yield:

: C₃₃H₄₁N₃O₆S₂

: 868836-20-8
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(4-tert-butyl)benzyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / dimethylformamide / 0.5 h / 0 °C

1.2: 71.6 percent / dimethylformamide / 12 h

2.1: 70.8 percent / hydrazine / methanol / 12 h / Heating

3.1: 78.3 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

4.1: 80 percent / aq. LiOH / tetrahydrofuran / 0 - 20 °C

With lithium hydroxide; sodium hydride; triethylamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0505009